Suppr超能文献

[采用8-羟基喹啉快速共沉淀技术预富集后火焰原子吸收光谱法测定啤酒中的铜和铅]

[Flame atomic absorption spectrometric determination of copper and lead in beer after preconcentration using a rapid coprecipitation technique with 8-oxyquinoline].

作者信息

Su Yao-dong, Hao Bing-bing, Qin Li-jun, Gan Li-hua

机构信息

Department of Chemistry, Tongji University, Shanghai 200092, China.

出版信息

Guang Pu Xue Yu Guang Pu Fen Xi. 2007 Mar;27(3):589-91.

Abstract

A method was proposed for the determination of trace copper and lead in beer with flame atomic absorption spectrometry after preconcentration of copper and lead by rapid coprecipitation technique with 8-oxyquinoline-Mg(II) using manganese as an internal standard at pH 9. The standard addition recovery of lead is between 97.6%-103.0%. The detection limit is 6.28 x 10(-3) microg x mL(-1) for copper and 2.26 x 10(-2) microg x mL(-1) for lead when the sample volume is 100 mL. The effect of matrix can be overcome by the method and the results are satisfying. The method proposed here is rapid and has good reproducibility.

摘要

提出了一种用火焰原子吸收光谱法测定啤酒中痕量铜和铅的方法。该方法在pH 9的条件下,以锰为内标,采用8-羟基喹啉-Mg(II)快速共沉淀技术对铜和铅进行预富集。铅的标准加入回收率在97.6%-103.0%之间。当样品体积为100 mL时,铜的检出限为6.28×10(-3) μg·mL(-1),铅的检出限为2.26×10(-2) μg·mL(-1)。该方法可克服基体效应,结果令人满意。所提出的方法快速且具有良好的重现性。

文献AI研究员

20分钟写一篇综述,助力文献阅读效率提升50倍。

立即体验

用中文搜PubMed

大模型驱动的PubMed中文搜索引擎

马上搜索

文档翻译

学术文献翻译模型,支持多种主流文档格式。

立即体验