Radovic Ivana, Monticelli Francesca, Papacchini Federica, Magni Elisa, Cury Alvaro Hafiz, Vulicevic Zoran R, Ferrari Marco
Clinic for Pediatric and Preventive Dentistry, Faculty of Dentistry, University of Belgrade, Dr. Subotica 11, Beograd 11000, Serbia.
J Dent. 2007 Aug;35(8):683-9. doi: 10.1016/j.jdent.2007.05.006. Epub 2007 Jul 5.
Although fiber posts luted in root canals are not directly exposed to oral fluids, water storage is considered as in vitro accelerated aging test for bonded interfaces. The aim of the study was to evaluate the influence of accelerated water aging on fiber post-resin composite adhesion.
Forty fiber posts (DT Light Post, RTD) were randomly divided into two main groups, according to the surface treatment performed. Group I: XPBond adhesive (Dentsply Caulk); Group II: sandblasting (Rocatec-Pre, 3M ESPE) and XPBond. Dual-cured resin cement (Calibra, Dentsply Caulk) and flowable composite (X-Flow, Dentsply Caulk) were applied on the posts to produce cylindrical specimens. The bond strength at the interface between post and cement/composite was measured with the microtensile test according to the non-trimming technique. Half of the sticks were tested immediately for bond strength, while in the other half testing was performed after 1 month of water storage at 37 degrees C. Post-cement/composite interfaces were evaluated under SEM prior and after water aging. Statistical analysis was performed using the Kruskal-Wallis ANOVA followed by Dunn's multiple range test (p<0.05).
Immediate bond strength was higher on sandblasted posts. After water aging the two post surface treatments resulted comparable in bond strength. Resin cement achieved higher bond strength to fiber posts than flowable composite. Water aging significantly reduced bond strength.
Sandblasting followed by adhesive coating may improve immediate post-resin bond strength in comparison to adhesive alone. However, fiber post-resin bond strength mediated by hydrophilic adhesive tends to decrease after water aging.
尽管根管内粘结的纤维桩未直接暴露于口腔液体中,但储水被视为粘结界面的体外加速老化试验。本研究的目的是评估加速水老化对纤维桩-树脂复合材料粘结的影响。
根据表面处理方式,将40根纤维桩(DT Light Post,RTD)随机分为两个主要组。第一组:XPBond粘结剂(登士柏卡沃);第二组:喷砂处理(Rocatec-Pre,3M ESPE)后使用XPBond。在桩上应用双固化树脂水门汀(Calibra,登士柏卡沃)和流动树脂复合材料(X-Flow,登士柏卡沃)制作圆柱形试件。根据非修整技术,通过微拉伸试验测量桩与水门汀/复合材料之间界面的粘结强度。一半试件立即测试粘结强度,另一半在37℃储水1个月后进行测试。在水老化前后,通过扫描电子显微镜对桩-水门汀/复合材料界面进行评估。采用Kruskal-Wallis方差分析和Dunn多重范围检验进行统计分析(p<0.05)。
喷砂处理的桩的即时粘结强度更高。水老化后,两种桩表面处理方式的粘结强度相当。树脂水门汀与纤维桩的粘结强度高于流动树脂复合材料。水老化显著降低了粘结强度。
与单独使用粘结剂相比,喷砂后进行粘结剂涂层处理可提高纤维桩与树脂的即时粘结强度。然而,由亲水性粘结剂介导的纤维桩-树脂粘结强度在水老化后趋于降低。