De Witte K, Cool P, De Witte I, Ruys L, Rao J, Van Tendeloo G, Vansant E F
Laboratory of Adsorption and Catalysis, University of Antwerpen, Universiteitsplein 1, B-2610 Wilrijk, Belgium.
J Nanosci Nanotechnol. 2007 Jul;7(7):2511-5. doi: 10.1166/jnn.2007.445.
A multistep deposition of anatase nanoparticles was employed to incorporate high amounts of titania into the mesopores of SBA-15. Anatase nanoparticles were synthesized and deposited following the Acid Catalyzed Sol Gel method. With this method, the size of the anatase nanoparticles can be controlled and therefore, the titania loading into the mesopores of SBA-15 can be controlled. Through multistep deposition of anatase nanoparticles, a further increase of titania loading into the mesoporous channels can be obtained. For the degradation of Rhodamine-6G, the samples synthesized by multistep deposition showed an enhanced photocatalytic activity.
采用锐钛矿型纳米颗粒的多步沉积法,将大量二氧化钛掺入SBA - 15的介孔中。按照酸催化溶胶 - 凝胶法合成并沉积锐钛矿型纳米颗粒。通过这种方法,可以控制锐钛矿型纳米颗粒的尺寸,从而可以控制二氧化钛在SBA - 15介孔中的负载量。通过锐钛矿型纳米颗粒的多步沉积,可以进一步提高介孔通道中二氧化钛的负载量。对于罗丹明 - 6G的降解,通过多步沉积合成的样品表现出增强的光催化活性。