Stafslien Shane J, Bahr James A, Daniels Justin W, Wal Lyndsi Vander, Nevins Jonathan, Smith Jeremy, Schiele Kris, Chisholm Bret
Center for Nanoscale Science and Engineering, North Dakota State University, 1805 NDSU Research Park Drive, Fargo, North Dakota 58102, USA.
Rev Sci Instrum. 2007 Jul;78(7):072204. doi: 10.1063/1.2755965.
Large numbers of coatings can be generated very quickly using a combinatorial high-throughput approach. Rapid screening assays are typically required to adequately evaluate and down select coating candidates to identify promising compositions. An automated, spinning water jet apparatus was developed to rapidly characterize the adhesion strength of marine organisms to coating surfaces. Coating arrays are cast in multiwell plates and subjected to a jet of water of controlled pressure and duration. Array plates are manipulated by a robotic arm to facilitate accurate and repeatable water jet treatments. Jet pressures of 40-688 kPa can be generated and precisely maintained by computer control. A five axis robotic arm selects plates from three plate stacking hotels yielding a total of 39 plates or 936 individual coating samples for each experimental run. All robotic instructions, process parameters, and data are stored and controlled by the computer. The large plate handling capacity offered by the robotic system enables the analysis of a wide variety of coatings for "fouling-release" properties. A brief example demonstrating the capability of the automated water jet apparatus to evaluate marine bacterial adhesion to coating surfaces is provided.
使用组合高通量方法可以非常快速地生成大量涂层。通常需要快速筛选试验来充分评估并筛选涂层候选物,以确定有前景的组合物。开发了一种自动旋转水射流装置,以快速表征海洋生物对涂层表面的附着强度。涂层阵列浇铸在多孔板中,并受到具有受控压力和持续时间的水流喷射。阵列板由机器人手臂操作,以促进精确且可重复的水射流处理。通过计算机控制可以产生并精确维持40 - 688 kPa的喷射压力。一个五轴机器人手臂从三个板堆叠架中选择板,每次实验运行总共产生39个板或936个单独的涂层样品。所有机器人指令、工艺参数和数据都由计算机存储和控制。机器人系统提供的大板处理能力使得能够分析各种具有“防污释放”特性的涂层。提供了一个简要示例,展示了自动水射流装置评估海洋细菌对涂层表面附着力的能力。