Department of Geology and Planetary Science, University of Pittsburgh, Pittsburgh, PA 15260, USA.
Geochem Trans. 2007 Oct 10;8:9. doi: 10.1186/1467-4866-8-9.
Standardized sample preparation techniques allow comparison of pyrite dissolution experiments under diverse conditions. Our objective was to assess dry and wet sieving preparation methodologies, and to develop a reproducible technique that yields uniformly size-distributed material within a limited size range of interest.
Here, we describe a wet sieving preparation method that successfully concentrates pyrite particles within a 44-75 microm diameter range. In addition, this technique does not require a post-processing cleanup step to remove adhering particles, as those particles are removed during the procedure. We show that sample preparation methods not only affect the pyrite size distribution, but also apparent dissolution rates.
The presented methodology is non-destructive to the sample, uses readily available chemical equipment within the laboratory, and could be applied to minerals other than pyrite.
标准化的样品制备技术可以在不同条件下比较黄铁矿溶解实验。我们的目标是评估干筛和湿筛制备方法,并开发一种可重复的技术,在有限的感兴趣的粒径范围内产生均匀分布的材料。
在这里,我们描述了一种湿筛制备方法,成功地将黄铁矿颗粒集中在 44-75 微米直径范围内。此外,该技术不需要进行后处理清洁步骤来去除附着的颗粒,因为这些颗粒在过程中被去除。我们表明,样品制备方法不仅影响黄铁矿的粒径分布,而且还影响明显的溶解速率。
所提出的方法对样品无损伤,使用实验室中现成的化学设备,并且可以应用于除黄铁矿以外的其他矿物。