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用于扫描探针扫描探针显微镜的摩擦力显微镜串扰效应的定量表征。

Quantitative characterization of crosstalk effects for friction force microscopy with scan-by-probe SPMs.

作者信息

Prunici Pavel, Hess Peter

机构信息

Institute of Physical Chemistry, University of Heidelberg, D-69120 Heidelberg, Germany.

出版信息

Ultramicroscopy. 2008 Jun;108(7):642-5. doi: 10.1016/j.ultramic.2007.10.001. Epub 2007 Oct 17.

Abstract

If the photodetector and cantilever of an atomic force microscope (AFM) are not properly adjusted, crosstalk effects will appear. These effects disturb measurements of the absolute vertical and horizontal cantilever deflections, which are involved in friction force microscopy (FFM). A straightforward procedure is proposed to study quantitatively crosstalk effects observed in scan-by-probe SPMs. The advantage of this simple, fast, and accurate procedure is that no hardware change or upgrade is needed. The results indicate that crosstalk effects depend not only on the alignment of the detector but also on the cantilever properties, position, and detection conditions. The measurements may provide information on the origin of the crosstalk effect. After determination of its magnitude, simple correction formulas can be applied to correct the crosstalk effects and then the single-load wedge method, using a commercially available grating, can be employed for accurate calibration of the lateral force.

摘要

如果原子力显微镜(AFM)的光电探测器和悬臂未正确调整,就会出现串扰效应。这些效应会干扰摩擦力显微镜(FFM)中所涉及的悬臂绝对垂直和水平偏转的测量。本文提出了一种直接的程序来定量研究在逐探针扫描式扫描探针显微镜(SPM)中观察到的串扰效应。这种简单、快速且准确的程序的优点在于无需对硬件进行更改或升级。结果表明,串扰效应不仅取决于探测器的对准情况,还取决于悬臂的特性、位置和检测条件。这些测量可以提供有关串扰效应起源的信息。在确定其大小之后,可以应用简单的校正公式来校正串扰效应,然后可以使用市售光栅的单负载楔形法来精确校准侧向力。

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