金属有机框架的一步固态热解：一种简单便捷的大规模制备多壁碳纳米管的方法。
One-step solid-state thermolysis of a metal-organic framework: a simple and facile route to large-scale of multiwalled carbon nanotubes.
作者信息
Chen Linyun, Bai Junfeng, Wang Chunzhao, Pan Yi, Scheer Manfred, You Xiaozeng
机构信息
State Key Laboratory of Coordination Chemistry, Department of Chemistry & Chemical Engineering, Nanjing University, Nanjing, China.
出版信息
Chem Commun (Camb). 2008 Apr 7(13):1581-3. doi: 10.1039/b718476j. Epub 2008 Jan 31.
We report a simple and facile solid-state approach to large-scale synthesis of multiwalled carbon nanotubes (MCNTs), for the first time, by one-step direct thermolysis of a metal-organic framework [Ni(3)(btc)(2).12H(2)O] (btc = benzene-1,3,5-tricarboxylato) in a one-end closed conventional horizontal tube furnace under relatively low temperature without using any additional carrier gas or catalyst.
我们首次报道了一种简单易行的固态方法，用于大规模合成多壁碳纳米管（MCNT），即在一端封闭的传统卧式管式炉中，在相对较低温度下，通过一步直接热解金属有机框架[Ni(3)(btc)(2).12H(2)O]（btc = 苯-1,3,5-三羧酸根）来实现，且无需使用任何额外的载气或催化剂。
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