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基于激光的原位技术:在透射电子显微镜(TEM)样品中产生极端条件的新方法。

Laser-based in situ techniques: novel methods for generating extreme conditions in TEM samples.

作者信息

Taheri Mitra L, Lagrange Thomas, Reed Bryan W, Armstrong Michael R, Campbell Geoffrey H, DeHope William J, Kim Judy S, King Wayne E, Masiel Daniel J, Browning Nigel D

机构信息

Chemistry, Materials, Earth & Life Sciences Directorate, Lawrence Livermore National Laboratory, Livermore, California, USA.

出版信息

Microsc Res Tech. 2009 Mar;72(3):122-30. doi: 10.1002/jemt.20664.

Abstract

The dynamic transmission electron microscope (DTEM) is introduced as a novel tool for in situ processing of materials. Examples of various types of dynamic studies outline the advantages and differences of laser-based heating in the DTEM in comparison to conventional (resistive) heating in situ TEM methods. We demonstrate various unique capabilities of the drive laser, namely, in situ processing of nanoscale materials, rapid and high temperature phase transformations, and controlled thermal activation of materials. These experiments would otherwise be impossible without the use of the DTEM drive laser. Thus, the potential of the DTEM as a new technique to process and characterize the growth of a myriad of micro and nanostructures is demonstrated.

摘要

动态透射电子显微镜(DTEM)作为一种用于材料原位处理的新型工具被引入。各种类型的动态研究示例概述了DTEM中基于激光加热与传统(电阻)加热原位TEM方法相比的优势和差异。我们展示了驱动激光的各种独特功能,即纳米级材料的原位处理、快速和高温相变以及材料的可控热激活。否则,不使用DTEM驱动激光,这些实验将无法进行。因此,证明了DTEM作为一种处理和表征众多微观和纳米结构生长的新技术的潜力。

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