Reilly Matthew A, Perry Gavin, Ravi Nathan
Research, Department of Veterans Affairs, St. Louis, Missouri 63106, USA.
Rev Sci Instrum. 2009 Jan;80(1):015105. doi: 10.1063/1.3043428.
We developed a microindentation instrument that allows direct measurement of the point of contact for reasonably conductive samples. This is achieved in the absence of a contact load using a simple electrical circuit. Force is measured using an optical interrupter to measure the deflection of a cantilever beam. Displacement is achieved using a piezoelectric motor and is measured using an independent optical interrupter. Force and displacement measurements are accomplished in real time, allowing the specification of arbitrary waveforms. The instrument was rigorously validated by comparing mechanical property measurements from the indenter with results from traditional dynamic mechanical analysis. Details of the construction and feedback control schemes are given explicitly.
我们开发了一种微压痕仪器,可对具有一定导电性的样品直接测量接触点。这是通过一个简单的电路在无接触载荷的情况下实现的。使用光学中断器测量悬臂梁的挠度来测定力。通过压电马达实现位移,并使用独立的光学中断器进行测量。力和位移测量实时完成,可设定任意波形。通过将压头的力学性能测量结果与传统动态力学分析结果进行比较,对该仪器进行了严格验证。文中明确给出了仪器构造及反馈控制方案的详细信息。