Reinhold M, Kiener D, Knowlton W B, Dehm G, Müllner P
J Appl Phys. 2009 Sep 1;106(5):53906. doi: 10.1063/1.3211327. Epub 2009 Sep 4.
The maximum actuation frequency of magnetic shape-memory alloys (MSMAs) significantly increases with decreasing size of the transducer making MSMAs interesting candidates for small scale actuator applications. To study the mechanical properties of Ni-Mn-Ga single crystals on small length scales, two single-domain micropillars with dimensions of 10x15x30 mum(3) were fabricated from a Ni-Mn-Ga monocrystal using dual beam focused ion beam machining. The pillars were oriented such that the crystallographic c direction was perpendicular to the loading direction. The pillars were compressed to maximum stresses of 350 and 50 MPa, respectively. Atomic force microscopy and magnetic force microscopy were performed prior to fabrication of the pillars and following the deformation experiments. Both micropillars were deformed by twinning as evidenced by the stress-strain curve. For one pillar, a permanent deformation of 3.6% was observed and ac twins (10M martensite) were identified after unloading. For the other pillar, only 0.7% remained upon unloading. No twins were found in this pillar after unloading. The recovery of deformation is discussed in the light of pseudoelastic twinning and twin-substrate interaction. The twinning stress was higher than in similar macroscopic material. However, further studies are needed to substantiate a size effect.
随着换能器尺寸减小,磁性形状记忆合金(MSMA)的最大驱动频率显著增加,这使得MSMA成为小规模致动器应用的有趣候选材料。为了在小长度尺度上研究Ni-Mn-Ga单晶的力学性能,使用双束聚焦离子束加工从Ni-Mn-Ga单晶制备了两个尺寸为10×15×30μm³的单畴微柱。微柱的取向使得晶体学c方向垂直于加载方向。微柱分别被压缩至350和50MPa的最大应力。在微柱制造之前和变形实验之后进行了原子力显微镜和磁力显微镜观察。如应力-应变曲线所示,两个微柱均通过孪生发生变形。对于其中一个微柱,观察到3.6%的永久变形,卸载后识别出a-c孪生(10M马氏体)。对于另一个微柱,卸载后仅保留0.7%。卸载后在该微柱中未发现孪生。根据伪弹性孪生和孪晶-基体相互作用讨论了变形的恢复情况。孪生应力高于类似宏观材料中的孪生应力。然而,需要进一步研究来证实尺寸效应。