Department of Prosthodontics, Propaedeutics and Dental Materials, Dental School, Christian-Albrechts University at Kiel, Arnold-Heller-Str. 16, 24105 Kiel, Germany.
Clin Oral Investig. 2011 Jun;15(3):383-91. doi: 10.1007/s00784-010-0394-x. Epub 2010 Mar 16.
The aim of this study was to evaluate the microstructural quality of noble alloy castings from commercial dental laboratories using the wiping-etching method as a simple method for quality control. In total, 240 castings from two noble alloys (AuAgCuPt and AuPtZn) were taken from a day's production of five different dental laboratories. The casting quality was evaluated by determining the grain size and by assessing the number and size of shrinkage cavities after acidic etching of the alloy surfaces. The AuAgCuPt alloy castings showed an acceptable quality in the microstructural analysis. The results of AuPtZn castings, however, were not satisfactory because 50.8% of the samples showed a remarkably poorer quality compared to the specifications made by the manufacturer. The proportion of the employed reclaimed alloy had no influence on the casting quality when AuAgCuPt alloy was used, but was influential when casting restorations with AuPtZn alloy. When determining the quantity and size of shrinkage cavities, none of the evaluated castings was of such a poor quality that a replacement of the castings had to be considered. The differences in grain size and quantity of shrinkage cavities were reflecting the individual laboratory process rather than the admixture of new/reclaimed alloy. The presented analysis can be used as a simple method for quality control of dental castings.
本研究旨在使用擦拭蚀刻法评估商业牙科实验室生产的贵金属合金铸件的微观结构质量,该方法作为一种简单的质量控制方法。共从五个不同牙科实验室一天的生产中取出 240 个 AuAgCuPt 和 AuPtZn 两种贵金属合金的铸件。通过确定晶粒尺寸以及在对合金表面进行酸性蚀刻后评估收缩腔的数量和大小来评估铸件质量。AuAgCuPt 合金铸件的微观结构分析结果可接受。然而,AuPtZn 合金铸件的结果并不令人满意,因为与制造商的规格相比,50.8%的样品显示出明显较差的质量。当使用 AuAgCuPt 合金时,回收合金的使用比例对铸件质量没有影响,但当铸造 AuPtZn 合金修复体时,会产生影响。在确定收缩腔的数量和大小时,没有一个评估的铸件质量差到需要更换铸件的程度。晶粒尺寸和收缩腔数量的差异反映了各个实验室的工艺,而不是新/回收合金的混合物。本分析可作为牙科铸件质量控制的简单方法。