Synthesis and Characterization of Rutile TiO(2) Nanopowders Doped with Iron Ions.

作者信息

Abazović Nadica D, Mirenghi Luciana, Janković Ivana A, Bibić Nataša, Sojić Daniela V, Abramović Biljana F, Comor Mirjana I

出版信息

Nanoscale Res Lett. 2009 Feb 28;4(6):518-525. doi: 10.1007/s11671-009-9274-1.

DOI:10.1007/s11671-009-9274-1

PMID:20596442

原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2893899/

Abstract

Titanium dioxide nanopowders doped with different amounts of Fe ions were prepared by coprecipitation method. Obtained materials were characterized by structural (XRD), morphological (TEM and SEM), optical (UV/vis reflection and photoluminescence, and Raman), and analytical techniques (XPS and ICP-OES). XRD analysis revealed rutile crystalline phase for doped and undoped titanium dioxide obtained in the same manner. Diameter of the particles was 5-7 nm. The presence of iron ions was confirmed by XPS and ICP-OES. Doping process moved absorption threshold of TiO(2) into visible spectrum range. Photocatalytic activity was also checked. Doped nanopowders showed normal and up-converted photoluminescence.

摘要