Department of Physics, College of Science, Shanghai University, Shanghai, China.
Talanta. 2010 Jul 15;82(2):458-63. doi: 10.1016/j.talanta.2010.04.053. Epub 2010 May 4.
SnO(2) nanowires with an average 0.6 microm in length and about 25 nm in diameter were prepared by a hydrothermal method. The sensors were fabricated using SnO(2) nanowires assembled with Pd nanocrystals. The sensing properties of the sensors such as selectivity, response-recovery time and stability were tested at 290 degrees C. After assembling Pd nanocrystals onto the surface of SnO(2) nanowires, the gas sensing properties of the sensors toward H(2)S were improved. The sensors based on Pd nanoparticle@SnO(2) nanowires exhibit high stability owing to stable single crystal structure. The mechanism of promoting sensing properties with Pd nanoparticles is discussed.
通过水热法制备了平均长度为 0.6 微米、直径约为 25nm 的 SnO(2)纳米线。传感器是使用组装有 Pd 纳米晶的 SnO(2)纳米线制成的。在 290°C 下测试了传感器的选择性、响应-恢复时间和稳定性等传感性能。在将 Pd 纳米晶组装到 SnO(2)纳米线表面后,传感器对 H(2)S 的气体传感性能得到了提高。基于 Pd 纳米颗粒@SnO(2)纳米线的传感器由于具有稳定的单晶结构,因此表现出高稳定性。讨论了 Pd 纳米颗粒促进传感性能的机制。