2-苯胺基-3-苯甲酰基-4-(2,5-二氯苯基)-7,7-二甲基-5-氧代-5,6,7,8-四氢-4H-苯并[b]吡喃
2-Anilino-3-benzoyl-4-(2,5-dichloro-phen-yl)-7,7-dimethyl-5-oxo-5,6,7,8-tetra-hydro-4H-benzo[b]pyran.
作者信息
Wen Li-Rong, Sun Ji-Hui, Ji Chen, Xie Huai-Yuan
机构信息
College of Chemistry and Molecular Engineering, Qingdao University of Science and Technology, Qingdao 266042, People's Republic of China.
出版信息
Acta Crystallogr Sect E Struct Rep Online. 2008 Jan 9;64(Pt 2):o407. doi: 10.1107/S1600536807068377.
The title compound, C(30)H(25)Cl(2)NO(3), was prepared by the reaction of 3-oxo-N,3-diphenyl-propane-thio-amide, 2,5-dichloro-benzaldehyde and 5,5-dimethyl-1,3-cyclo-hexa-nedione (1:1:1) in ethanol. The cyclohexene ring adopts a half-chair conformation. The crystal structure exhibits intra-molecular N-H⋯O and C-H⋯O, and inter-molecular C-H⋯O inter-actions.
标题化合物C(30)H(25)Cl(2)NO(3)是由3-氧代-N,3-二苯基丙硫酰胺、2,5-二氯苯甲醛和5,5-二甲基-1,3-环己二酮（1:1:1）在乙醇中反应制得。环己烯环呈半椅式构象。晶体结构显示出分子内的N-H⋯O和C-H⋯O相互作用以及分子间的C-H⋯O相互作用。
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