Johnston Andrea, Florence Alastair J, Fabbiani Francesca J A, Shankland Kenneth, Bedford Colin T
Acta Crystallogr Sect E Struct Rep Online. 2008 Jun 19;64(Pt 7):o1295-6. doi: 10.1107/S1600536808018059.
Cytenamide forms a 1:1 solvate with butyric acid [systematic name: 5H-dibenzo[a,d]cyclo-hepta-triene-5-carboxamide-butanoic acid (1/1)], C(16)H(13)NO·C(4)H(8)O(2). The title compound crystallizes with one mol-ecule of cytenamide and one of butyric acid in the asymmetric unit; these mol-ecules are linked by N-H⋯O and O-H⋯O hydrogen bonds to form an R(2) (2)(8) heterodimer motif. Pairs of adjacent motifs are further connected via N-H⋯O inter-actions to form a discrete centrosymmetric assembly.
胞嘧啶酰胺与丁酸形成1:1溶剂化物[系统名称:5H-二苯并[a,d]环庚三烯-5-甲酰胺-丁酸(1/1)],C(16)H(13)NO·C(4)H(8)O(2)。标题化合物在不对称单元中由一个胞嘧啶酰胺分子和一个丁酸分子结晶;这些分子通过N-H⋯O和O-H⋯O氢键相连,形成R(2) (2)(8)异二聚体基序。相邻基序对通过N-H⋯O相互作用进一步连接,形成一个离散的中心对称聚集体。