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N-Benzoyl-N'-(2-chloro-3-pyrid-yl)thio-urea.

作者信息

Ding Yu-Jie, Yao Jian, Wu Jian-Chao, Dong Wen-Kui, Tong Jun-Feng

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Jul 18;65(Pt 8):o1903. doi: 10.1107/S1600536809027081.

Abstract

The title compound, C(13)H(10)ClN(3)OS, was prepared by the reaction of 3-amino-2-chloropyridine with benzoyl isothio-cyanate at room temperature. The thio-urea group makes dihedral angles of 47.17 (5) and 51.88 (4)°, respectively, with the benzene and pyridyl rings, while the angle between the benzene and pyridine rings is 8.91 (3)°. Inter-molecular hydrogen-bond inter-actions link neighbouring mol-ecules into an infinite supra-molecular structure.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/84c5/2977241/e60518b60ce4/e-65-o1903-fig1.jpg

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