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引起 Jutrzenka 利口酒香气的挥发性化合物。

Volatile compounds responsible for aroma of Jutrzenka liquer wine.

机构信息

Faculty of Food Science and Nutrition, Poznań University of Life Sciences, Wojska Polskiego 31, 60-624 Poznań, Poland.

出版信息

J Chromatogr A. 2011 Oct 21;1218(42):7566-73. doi: 10.1016/j.chroma.2011.07.023. Epub 2011 Jul 20.

Abstract

Jutrzenka is a sweet liquer wine produced in Poland from the grape variety of the same name, developed in Poland to withstand the harsh climate of winery regions. Jutrzenka wine has a characteristic aroma with strong fruity and flowery notes, which make it unique among other liquer wines as demonstrated in sensory profile analysis. The work was aimed at characterization of volatile compounds in this wine, with the emphasis on characterization of compounds responsible for its unique aroma. Gas chromatography-olfactometry (GC-O) was applied to identify the key odorants using aroma extract dilution analysis (AEDA) approach. To facilitate free and bound terpenes and C(13)-norisoprenoids identification solid phase extraction (SPE) was used followed by GC/MS. Among identified key odorants β-damascenone was the compound having the highest FD (4096), followed by isoamyl alcohol, 4-mercapto-4-methyl-2-pentanone (FD=2048), methional, linalool, ethyl decanoate (FD=1024) and ethyl hexanoate, furaneol (FD=512). Other significant compounds were ethyl 2-methyl propanoate, ethyl 2-methylbutanoate and phenyl ethyl alcohol. Determination of odor activity values (OAV) showed the highest values for β-damascenone (566), 4-mercapto-4-methyl-2-pentanone (288) ethyl hexanoate (32) and linalool (7). Jutrzenka exhibited also a rich profile of free, and to lesser extent bound terpenes.

摘要

尤特津卡是一种在波兰生产的甜利口酒,采用同名葡萄品种酿造,专为波兰各葡萄酒产区的恶劣气候而开发。尤特津卡葡萄酒具有独特的香气,带有浓郁的果香和花香,在感官特征分析中表现出其在其他利口酒中的独特性。该研究旨在对这种葡萄酒中的挥发性化合物进行特征描述,重点是鉴定其独特香气的化合物。采用气相色谱-嗅觉测量法(GC-O)通过香气萃取稀释分析(AEDA)方法,对关键气味物质进行鉴定。为了便于游离萜烯和 C(13)-异戊二烯类物质的鉴定,采用固相萃取(SPE),然后进行 GC/MS 分析。在鉴定出的关键气味物质中,β-大马酮(FD=4096)的含量最高,其次是异戊醇、4-巯基-4-甲基-2-戊酮(FD=2048)、甲硫醇、芳樟醇、癸酸乙酯(FD=1024)和己酸乙酯、糠醇(FD=512)。其他重要的化合物还有 2-甲基丙酸乙酯、2-甲基丁酸乙酯和苯乙醇。气味活度值(OAV)的测定表明,β-大马酮(566)、4-巯基-4-甲基-2-戊酮(288)、己酸乙酯(32)和芳樟醇(7)的含量最高。尤特津卡还具有丰富的游离萜烯,以及较少的结合萜烯。

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