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新型甲基丙烯酸酯单体纳米杂化复合材料基体组成的机械稳定性。

The mechanical stability of nano-hybrid composites with new methacrylate monomers for matrix compositions.

机构信息

Department of Restorative Dentistry, Dental School of the Ludwig-Maximilians-University, Goethestr. 70, 80336 Munich, Germany.

出版信息

Dent Mater. 2012 Feb;28(2):152-9. doi: 10.1016/j.dental.2011.11.007. Epub 2011 Dec 3.

Abstract

OBJECTIVES

Dimer acid based metacrylates and TCD-urethane are promoted as new monomers of nano-hybrid resin based composites as alternatives for the conventional BisGMA. Investigations of this study focused on the mechanical and the storage behavior of nano-hybrid resin based composites (RBCs) composed of these new types of monomers in comparison to RBCs using BisGMA.

METHODS

Flexural strength and modulus were determined in a three-point-bending test. Additionally, the modulus of elasticity was measured on microscopic scale (E(micro)) using an automatic microhardness indenter. Tests were performed on samples after 24 h storage in distilled water, as well as after thermocycling and storing the materials for four weeks in either distilled water, artificial saliva or ethanol.

RESULTS

The six measured materials showed a pronounced decrease of flexural strength, flexural modulus and E(micro) after four weeks storage in alcohol. Results after four weeks storage in water and saliva could not be proven to be significantly different. The most sensitive factor of influence on all test parameters was the material.

SIGNIFICANCE

Nano-hybrid composites with new or conventional monomers performed similar in regard to the mechanical properties and the behavior of the materials after aging.

摘要

目的

二聚酸基甲基丙烯酸酯和 TCD-尿烷作为新型纳米复合树脂基单体被推广,作为传统 BisGMA 的替代品。本研究的重点是研究这些新型单体组成的纳米复合树脂基复合材料(RBC)的机械性能和储存性能,与使用 BisGMA 的 RBC 进行比较。

方法

在三点弯曲试验中测定弯曲强度和模量。此外,还使用自动显微硬度压痕计在微观尺度上测量弹性模量(E(micro))。在 24 小时储存在蒸馏水中以及在热循环和将材料在蒸馏水中、人工唾液或乙醇中储存四周后,对样品进行测试。

结果

六种测试材料在酒精中储存四周后,弯曲强度、弯曲模量和 E(micro)明显下降。在水中和唾液中储存四周后的结果不能证明有显著差异。对所有测试参数影响最敏感的因素是材料。

意义

具有新型或传统单体的纳米复合树脂在老化后,其机械性能和材料性能表现相似。

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