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(Nitrato-κO,O')bis-(tryptanthrin-κN)silver(I).

作者信息

Wu Jie, Huang Chao, Li Guo-Qiang, Tian Hai-Yan, Jiang Ren-Wang

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2012 Feb 1;68(Pt 2):m185-6. doi: 10.1107/S1600536812001821. Epub 2012 Jan 21.

Abstract

In the crystal structure of the title compound, [Ag(NO(3))(C(15)H(8)N(2)O(2))(2)], tryptanthrin (indolo[2,1-b]quinazoline-6,12-dione) and silver nitrate form a 2:1 complex. The silver ion is surrounded by two tryptanthrin ligands, each coordinating through the N atoms, with Ag-N bond lengths of 2.247 (3) and 2.264 (3) Å, and an anionic nitrate ligand coordinating through two O atoms, with Ag-O bond lengths of 2.499 (3) and 2.591 (3) Å. The N-Ag-N plane and the O-Ag-O plane are roughly perpendicular, making a dihedral angle of 81.6 (2)°. In the crystal, C-H⋯O inter-actions between aromatic H atoms and keto and nitrate O atoms as well as π-π inter-actions [centroid-centroid distance = 3.706 (4) Å] give rise to a three-dimensional network.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/59ec/3274910/d76efed90536/e-68-0m185-fig1.jpg

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Cell Mol Immunol. 2009 Oct;6(5):335-42. doi: 10.1038/cmi.2009.44.
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Isolation, structure elucidation, and synthesis of cytotoxic tryptanthrin analogues from Phaius mishmensis.
J Nat Prod. 2008 Jul;71(7):1275-9. doi: 10.1021/np800064w. Epub 2008 May 29.
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