3-Nitro-N-[(pyrrolidin-1-yl)carbothioyl]benzamide.
作者信息
Zulkifli Nursakinah, Yusoff Siti Fairus M, Yamin Bohari M
机构信息
School of Chemical Sciences and Food Technology, Universiti Kebangsaan Malaysia, 43600 Bangi, Selangor, Malaysia.
出版信息
Acta Crystallogr Sect E Struct Rep Online. 2012 Jun 1;68(Pt 6):o1785. doi: 10.1107/S1600536812021319. Epub 2012 May 19.
Abstract
In the mol-ecule of the title compound, C(12)H(13)N(3)O(3)S, the pyrrolidine ring adopts a half-chair conformation and the dihedral angle formed by the nitro group with the benzene ring is 15.18 (18)°. In the crystal, mol-ecules are linked by N-H⋯S and C-H⋯O inter-molecular hydrogen bonds into chains parallel to the c axis.
摘要
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1
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2
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