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Ethyl 2-acet-amido-4,5,6,7-tetra-hydro-1-benzothio-phene-3-carboxyl-ate.

作者信息

Mukhtar Asma, Tahir M Nawaz, Khan Misbahul Ain, Ather Abdul Qayyum, Khan Muhammad Naeem

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2012 Jul 1;68(Pt 7):o2042. doi: 10.1107/S160053681202524X. Epub 2012 Jun 13.

Abstract

In the title compound, C(13)H(17)NO(3)S, the dihedral angles between the thio-phene ring and the ethyl ester and acetamide groups are 5.21 (13) and 10.06 (16)°, respectively. The cyclo-hezene ring adopts a half-chair conformation. An S(6) ring is formed due to an intra-molecular N-H⋯O hydrogen bond. In the crystal, mol-ecules are linked by C-H⋯O inter-actions between the tetra-hydro-1-benzothio-phene unit and the ethyl ester group, forming C(7) chains propagating along the b-axis direction.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ac3e/3393310/dcd0538d0563/e-68-o2042-fig1.jpg

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