Chemical Engineering Department, Campus of Rabanales, Building Marie Curie (C-3), University of Córdoba, 14071 Córdoba, Spain.
Bioresour Technol. 2013 Mar;132:115-20. doi: 10.1016/j.biortech.2012.12.189. Epub 2013 Jan 11.
Influence of operational variables in the EFB pulping [acetic acid (60-95%), hydrochloric acid (0.10-0.25%) and time (60-180 min)], on the yield, drainability or beating grade, Kappa number, lignin and viscosity of pulps was studied. By using a factorial design, equations were obtained that reproduced the experimental results for the dependent variables with errors less than 9-18%. These equations can be used to find the suitable conditions, so that operating with not too high values of operating variables (with minor costs of operation and capital) pulps with acceptable properties could be obtained: operating with 86.25% acetic acid, 0.25% hydrochloric acid and 120 min time, produced pulps with 46.56% yield, 15.9 °SR drainability, 36.3 Kappa number, 10.3% lignin and 303 mL/g viscosity, values all of them close to the optimal predicted.
研究了操作变量(乙酸(60-95%)、盐酸(0.10-0.25%)和时间(60-180 分钟))对 EFB 制浆[得率、滤水性或打浆度、卡伯值、木质素和纸浆粘度的影响。通过使用析因设计,获得了能够用误差小于 9-18%重现实验结果的方程。这些方程可用于寻找合适的条件,以便在操作变量(操作和资本成本较低)不太高的情况下获得具有可接受性能的纸浆:用 86.25%的乙酸、0.25%的盐酸和 120 分钟的时间操作,可得到 46.56%的得率、15.9°SR 的滤水性、36.3 的卡伯值、10.3%的木质素和 303 mL/g 的粘度,所有这些值都接近最佳预测值。