Selvamuthukumaran Meenakshisundaram, Khanum Farhath
Biochemistry & Nutrition Division, Defence Food Research Laboratory, Siddartha Nagar, Mysore, 570 011 Karnataka India.
J Food Sci Technol. 2014 Dec;51(12):3731-9. doi: 10.1007/s13197-012-0901-y. Epub 2012 Dec 11.
The response surface methodology was used to optimize the spray drying process for development of seabuckthorn fruit juice powder. The independent variables were different levels of inlet air temperature and maltodextrin concentration. The responses were moisture, solubility, dispersibility, vitamin C and overall color difference value. Statistical analysis revealed that independent variables significantly affected all the responses. The Inlet air temperature showed maximum influence on moisture and vitamin C content, while the maltodextrin concentration showed similar influence on solubility, dispersibility and overall color difference value. Contour plots for each response were used to generate an optimum area by superimposition. The seabuckthorn fruit juice powder was developed using the derived optimum processing conditions to check the validity of the second order polynomial model. The experimental values were found to be in close agreement to the predicted values and were within the acceptable limits indicating the suitability of the model in predicting quality attributes of seabuckthorn fruit juice powder. The recommended optimum spray drying conditions for drying 100 g fruit juice slurry were inlet air temperature and maltodextrin concentration of 162.5 °C and 25 g, respectively. The spray dried juice powder contains higher amounts of antioxidants viz., vitamin C, vitamin E, total carotenoids, total anthocyanins and total phenols when compared to commercial fruit juice powders and they are also found to be free flowing without any physical alterations such as caking, stickiness, collapse and crystallization by exhibiting greater glass transition temperature.
采用响应面法对沙棘果汁粉喷雾干燥工艺进行优化。自变量为不同水平的进风温度和麦芽糊精浓度。响应值为水分、溶解度、分散性、维生素C和总色差。统计分析表明,自变量对所有响应值均有显著影响。进风温度对水分和维生素C含量影响最大,而麦芽糊精浓度对溶解度、分散性和总色差的影响相似。通过叠加各响应值的等高线图来确定最佳区域。利用得出的最佳工艺条件制备沙棘果汁粉,以检验二阶多项式模型的有效性。实验值与预测值高度吻合,且在可接受范围内,表明该模型适用于预测沙棘果汁粉的品质特性。喷雾干燥100g果汁浆料的推荐最佳条件为进风温度162.5℃、麦芽糊精浓度25g。与市售果汁粉相比,喷雾干燥的果汁粉含有更高含量的抗氧化剂,即维生素C、维生素E、总类胡萝卜素、总花青素和总酚类物质,且由于具有较高的玻璃化转变温度,该果汁粉具有良好的流动性,无结块、发黏、塌陷和结晶等物理变化。