不对称3,6-分支甘露糖五糖的合成：一锅法连续糖基化与逐步合成的比较。
Synthesis of unsymmetrical 3,6-branched Man5 oligosaccharide: a comparison between one-pot sequential glycosylation and stepwise synthesis.
作者信息
Zhang Yan, Chen Congcong, Jin Lan, Tan Haining, Wang Fengshan, Cao Hongzhi
机构信息
National Glycoengineering Research Center, School of Pharmaceutical Science, Shandong University, Jinan 250012, China.
National Glycoengineering Research Center, School of Pharmaceutical Science, Shandong University, Jinan 250012, China; Key Laboratory of Chemical Biology (Ministry of Education), Shandong University, Jinan 250012, China.
出版信息
Carbohydr Res. 2015 Jan 12;401:109-14. doi: 10.1016/j.carres.2014.09.010. Epub 2014 Nov 15.
An expeditious three-component, one-pot sequential glycosylation protocol has been developed for the preparation of 3,6-branched unsymmetrical mannopentaose (Man5), employing a mannose trisaccharide donor, a mannose monosaccharide donor and a mannose monosaccharide acceptor. The high efficiency of this one-pot procedure was demonstrated by comparison study with a stepwise synthesis using the same three building blocks.
已经开发出一种快速的三组分一锅法连续糖基化方案，用于制备3,6-分支不对称甘露五糖（Man5），该方案使用一种甘露糖三糖供体、一种甘露糖单糖供体和一种甘露糖单糖受体。通过与使用相同三种构建模块的逐步合成进行比较研究，证明了这种一锅法的高效率。
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