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染色和漂白后漂白色度树脂基复合材料颜色变化的分光光度评估。

Spectrophotometric evaluation of color changes of bleach-shade resin-based composites after staining and bleaching.

作者信息

Farah Rafat Ibrahim, Elwi Hytham

机构信息

Assistant Professor, Department of Prosthodontics, Qassim University, Kingdom of Saudi Arabia, e-mail:

Assistant Professor, Department of Prosthodontics, Qassim University, Kingdom of Saudi Arabia.

出版信息

J Contemp Dent Pract. 2014 Sep 1;15(5):587-94. doi: 10.5005/jp-journals-10024-1584.

Abstract

UNLABELLED

Spectrophotometric evaluation of color changes of Bleach-shade resin-based composites after staining and bleaching.

AIM

The aim of this study was to evaluate the color stability of two commercially available bleach-shade resin composites (RC) after exposure to 3 storage solutions and the effect of 3 bleaching agents on the color stability and stain removal from stained RC.

MATERIALS AND METHODS

Two bleach-shade RC were evaluated in this study, including a nanoflled RC, Filtek(TM) Z350 XT (FZ), and a nanohybrid RC, Tetric(®) N-Ceram (TC), in the extra-white body (shade) (XWB) and L shades, respectively. Twenty-seven disk-shaped specimens, each measuring 12 mm in diameter and 2 mm in thickness, were prepared for each RC, with a total of 54 specimens. Specimens were randomly allocated into 3 groups of 9 specimens each and immersed in 3 storage solutions (distilled water, tea and coffee) for 7 days period. The 9 specimens in each staining group were further divided into 3 subgroups. Specimens in each subgroup (n = 3) were bleached using one of the bleaching agents (10 and 16% Zoom NiteWhite amorphous calcium phosphate (ACP), and Zoom 2 chairside with light activation) for 5 days period. The specimen colors were measured with spectrophotometer. The measurements were performed on each sample three times at baseline, after staining, and after bleaching. Color was expressed using the commission international de I'Eclairage (CIE) Lab* color space. The color differences (ΔE) between the three measurements were calculated and the results were statistically analyzed using Two-way and Three-way analysis of variance (ANOVA) and Tukey's posthoc tests. Level of significance was set at p < 0.05.

RESULTS

Tetric(®) N-ceram materials demonstrated significantly less color change than the FZ and the color change, which was greater after storage in coffee compared to tea, was statistically significant. The bleaching agents significantly influence the color changes of composite specimens. All groups showed (ΔE) values below 3.3 after bleaching, except for 'Zoom 2 chairside' with light activation groups, which is shown clinically unacceptable lighter shade (ΔE >3.3).

CONCLUSION

Bleach-shade composites showed significant discoloration (ΔE > 3.3) after being immersed into coffee and tea solutions. Nanoflled composites discolored more than nano-hybrid composites, and carbamide peroxide-based bleaching agents were effective in reducing the discoloration to a clinically acceptable value (ΔE > 3.3).

摘要

未标记

漂白色调树脂基复合材料染色和漂白后颜色变化的分光光度评估

目的

本研究旨在评估两种市售漂白色调树脂复合材料(RC)在暴露于3种储存溶液后的颜色稳定性,以及3种漂白剂对染色RC的颜色稳定性和污渍去除效果的影响。

材料与方法

本研究评估了两种漂白色调的RC,分别是纳米填充的RC,Filtek™ Z350 XT(FZ),以及纳米混合RC,Tetric® N-Ceram(TC),分别为超白色(色调)(XWB)和L色调。每种RC制备27个圆盘形试样,每个直径12mm,厚度2mm,共54个试样。试样随机分为3组,每组9个试样,浸入3种储存溶液(蒸馏水、茶和咖啡)中7天。每个染色组的9个试样进一步分为3个亚组。每个亚组(n = 3)的试样使用一种漂白剂(10%和16%的Zoom NiteWhite无定形磷酸钙(ACP),以及带光活化的椅旁Zoom 2)漂白5天。用分光光度计测量试样颜色。在基线、染色后和漂白后对每个样品进行3次测量。颜色使用国际照明委员会(CIE)Lab*颜色空间表示。计算三次测量之间颜色差异(ΔE),并使用双向和三向方差分析(ANOVA)以及Tukey事后检验对结果进行统计分析。显著性水平设定为p < 0.05。

结果

Tetric® N-ceram材料的颜色变化明显小于FZ,并且与茶相比,在咖啡中储存后颜色变化更大,具有统计学意义。漂白剂显著影响复合材料试样的颜色变化。除了带光活化的“椅旁Zoom 2”组外,所有组漂白后的(ΔE)值均低于3.3,该组显示出临床上不可接受的更浅色调(ΔE > 3.3)。

结论

漂白色调复合材料浸入咖啡和茶溶液后出现明显变色(ΔE > 3.3)。纳米填充复合材料的变色比纳米混合复合材料更严重,基于过氧化脲的漂白剂在将变色降低到临床上可接受的值(ΔE > 3.3)方面是有效的。

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