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I类洞现有黏结剂的评估:使用光学相干断层扫描和微拉伸黏结强度的无损成像

Assessment of current adhesives in class I cavity: Nondestructive imaging using optical coherence tomography and microtensile bond strength.

作者信息

Makishi Patricia, Thitthaweerat Suppason, Sadr Alireza, Shimada Yasushi, Martins Adriano Luis, Tagami Junji, Giannini Marcelo

机构信息

Dental Materials Division, Department of Restorative Dentistry, Piracicaba Dental School, State University of Campinas, Piracicaba, SP, Brazil.

Department of Operative Dentistry and Endodontics, Faculty of Dentistry, Mahidol University, Bangkok, Thailand.

出版信息

Dent Mater. 2015 Sep;31(9):e190-200. doi: 10.1016/j.dental.2015.06.013. Epub 2015 Jul 14.

Abstract

OBJECTIVES

To evaluate the sealing ability and the microtensile bond strength (MTBS) of different adhesive systems bonded to dentin in class I cavities.

METHODS

Round tapered dentin cavities (3-mm diameter, 1.5-mm height) prepared in extracted human molars were restored using composite resin (Clearfil Majesty Posterior) with two-step etch-and-rinse adhesive system (Adper Single Bond 2: ASB2), two-step self-etch adhesive (Clearfil SE Bond: CSEB), all-in-one adhesives (G-Bond Plus: GBP; Tri-S Bond Plus: TSBP), or no adhesive (Control), or bonded using low-shrinkage composite with its proper adhesive (Filtek Silorane, Silorane Adhesive System: FSS). After 24-h water storage or 10,000 cycles of thermal stress, the specimens were immersed into a contrast agent. Two and three-dimensional images were obtained using optical coherence tomography (OCT). The mean percentage of high brightness (HB%) at the interfacial zone in cross-sectional images was calculated as an indicator of contrast agent or gap at the interface. The specimens were then sectioned into beams and the MTBS measured.

RESULTS

The HB% (ASB2=TSBP=CSEB<FSS=GBP) and MTBS (CSEB=ASB2, CSEB>TSBP=GBP=FSS, ASB2>FSS) differed significantly among the adhesives. After aging, HB% increased for GBP and FSS specimens, and the MTBS decreased for FSS specimens (ANOVA, Tukey's post hoc, p<0.05). The HB% and MTBS were significantly and negatively correlated (p=0.002). Confocal laser scanning and scanning electron micrographs confirmed contrast agent infiltration within the gap.

SIGNIFICANCE

There was a significant correlation between sealing performance and bond strength of the adhesives in the whole cavity. After aging, the two-step systems showed equal or superior performance to the all-in-one and Silorane systems.

摘要

目的

评估不同粘接系统与I类洞型牙本质粘接后的封闭能力和微拉伸粘接强度(MTBS)。

方法

在拔除的人类磨牙上制备圆形锥形牙本质洞(直径3mm,高1.5mm),使用复合树脂(Clearfil Majesty Posterior)和两步酸蚀冲洗粘接系统(Adper Single Bond 2:ASB2)、两步自酸蚀粘接剂(Clearfil SE Bond:CSEB)、一步法粘接剂(G-Bond Plus:GBP;Tri-S Bond Plus:TSBP)进行修复,或不使用粘接剂(对照组),或使用低收缩复合树脂及其配套粘接剂(Filtek Silorane,Silorane粘接系统:FSS)进行粘接。在24小时水储存或10000次热循环后,将标本浸入造影剂中。使用光学相干断层扫描(OCT)获得二维和三维图像。计算横截面图像中界面区高亮度(HB%)的平均百分比,作为界面处造影剂或间隙的指标。然后将标本切成梁状并测量MTBS。

结果

粘接剂之间的HB%(ASB2=TSBP=CSEB<FSS=GBP)和MTBS(CSEB=ASB2,CSEB>TSBP=GBP=FSS,ASB2>FSS)存在显著差异。老化后,GBP和FSS标本的HB%增加,FSS标本的MTBS降低(方差分析,Tukey事后检验,p<0.05)。HB%和MTBS呈显著负相关(p=0.002)。共聚焦激光扫描和扫描电子显微镜照片证实造影剂渗入间隙内。

意义

在整个窝洞中,粘接剂的封闭性能和粘接强度之间存在显著相关性。老化后,两步法系统表现出与一步法和Silorane系统相当或更优的性能。

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