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大容量、低截留惯性冲击器的研制与验证

Development and Validation of a High-Volume, Low-Cutoff Inertial Impactor.

作者信息

Kavouras I G, Ferguson S T, Wolfson J M, Koutrakis P

机构信息

a Environmental Science and Engineering Program, Department of Environmental Health, School of Public Health , Harvard University , Boston , Massachusetts , USA.

出版信息

Inhal Toxicol. 2000 Jan;12 Suppl 2:35-50. doi: 10.1080/08958378.2000.11463198.

Abstract

A low-cutoff, high-volume conventional impactor has been designed. This sampler uses a slit-shaped acceleration jet and operates at 1100 L/min. The impaction substrate is polyurethane foam (PUF). The impactor collection efficiency was characterized using polydisperse particles, and the 50% size cutoff point was 0.12 ¡m. Losses within the sampler were also characterized and were less than 10%. The use of polyurethane foam (PUF) as a substrate has the following advantages: (I) PUF has a very high particle collection efficiency over a large range of particle sizes, even under conditions of heavy particle loading, as compared to other impaction substrates, such as flat plates and less porous membranes, which typically are subject to significant bounce-off and reentrainment; (2) no oil or grease coating is required, so potential interferences of impurities within such coatings are avoided when chemical, biological, and toxicological tests are performed on the collected particles; (3) PUF itself is chemically inert, minimizing interference with any of these tests; (4) because of the high flow rate of 1100 L/min, a large amount of particles can be collected in a short period of time on a relatively small surface of substrate, facilitating recovery of the collected particles for the different tests; and (5) a large amount of particles can be collected on a relatively small collection surface and easily extracted with small amounts of water or organic solvents. This method will be suitable for the collection of large amounts for toxicological studies and analysis of organic aerosols, which is not possible with other high-volume samplers that utilize large filtration surfaces.

摘要

已设计出一种低截留粒径、大容量的传统撞击式采样器。该采样器采用狭缝形加速喷嘴,运行流量为1100升/分钟。撞击衬底为聚氨酯泡沫(PUF)。使用多分散颗粒对撞击器的收集效率进行了表征,50%粒径截留点为0.12微米。还对采样器内部的损失进行了表征,损失小于10%。使用聚氨酯泡沫(PUF)作为衬底具有以下优点:(1)与其他撞击衬底(如平板和孔隙率较低的膜)相比,PUF在很宽的粒径范围内具有非常高的颗粒收集效率,即使在颗粒负载较重的情况下也是如此,而平板和孔隙率较低的膜通常会出现大量反弹和再夹带现象;(2)无需涂油或油脂,因此在对收集到的颗粒进行化学、生物和毒理学测试时,可避免此类涂层中杂质的潜在干扰;(3)PUF本身化学性质惰性,可将对任何此类测试的干扰降至最低;(4)由于流量高达1100升/分钟,可在较短时间内在相对较小的衬底表面上收集大量颗粒,便于为不同测试回收收集到的颗粒;(5)可在相对较小的收集表面上收集大量颗粒,并易于用少量水或有机溶剂提取。该方法适用于收集大量用于毒理学研究和有机气溶胶分析的样品,这是其他利用大过滤表面的大容量采样器所无法做到的。

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