Doozandeh Maryam, Alavi Ali Asghar, Karimizadeh Zahra
Dept. of Operative Dentistry, School of Dentistry, Shiraz University of Medical Sciences, Shiraz, Iran.
Dept. of Operative Dentistry and Biomaterials Research Center, School of Dentistry, Shiraz University of Medical Sciences, Shiraz, Iran.
J Dent (Shiraz). 2016 Jun;17(2):105-11.
Sufficient adhesion between silorane/methacrylate-based composites and methacrylate impregnated glass fiber increases the benefits of fibers and enhances the mechanical and clinical performance of both composites.
The aim of this study was to evaluate the compatibility of silorane and methacrylate-based composites with pre-impregnated glass fiber by using flexural strength (FS) test.
A total of 60 bar specimens were prepared in a split mold (25×2×2 mm) in 6 groups (n=10). In groups 1 and 4 (control), silorane-based (Filtek P90) and nanohybrid (Filtek Z350) composites were placed into the mold and photopolymerized with a high-intensity curing unit. In groups 2 and 5, pre-impregnated glass fiber was first placed into the mold and after two minutes of curing, the mold was filled with respective composites. Prior to filling the mold in groups 3 and 6, an intermediate adhesive layer was applied to the glass fiber. The specimens were stored in distilled water for 24 hours and then their flexural strength was measured by 3 point bending test, using universal testing machine at the crosshead speed of 1 mm/min. Two-way ANOVA and post-hoc test were used for analyzing the data (p< 0.05).
A significant difference was observed between the groups (p< 0.05). The highest FS was registered for combination of Z350 composite, impregnated glass fiber, and application of intermediate adhesive layer .The lowest FS was obtained in Filtek P90 alone. Cohesive failure in composite was the predominant failure in all groups, except group 5 in which adhesive failure between the composite and fiber was exclusively observed.
Significant improvement in FS was achieved for both composites with glass fiber. Additional application of intermediate adhesive layer before composite build up seems to increase FS. Nanohybrid composite showed higher FS than silorane-based composite.
硅氧烷/甲基丙烯酸酯基复合材料与甲基丙烯酸酯浸渍玻璃纤维之间的充分粘合增加了纤维的益处,并增强了两种复合材料的机械性能和临床性能。
本研究的目的是通过弯曲强度(FS)测试评估硅氧烷和甲基丙烯酸酯基复合材料与预浸渍玻璃纤维的相容性。
在分型模具(25×2×2mm)中制备6组共60个条形试样(n = 10)。在第1组和第4组(对照组)中,将硅氧烷基(Filtek P90)和纳米混合(Filtek Z350)复合材料放入模具中,并用高强度固化单元进行光聚合。在第2组和第5组中,首先将预浸渍玻璃纤维放入模具中,固化两分钟后,用相应的复合材料填充模具。在第3组和第6组填充模具之前,在玻璃纤维上施加中间粘合剂层。将试样在蒸馏水中储存24小时,然后使用万能试验机以1mm/min的十字头速度通过三点弯曲试验测量其弯曲强度。使用双向方差分析和事后检验分析数据(p < 0.05)。
各组之间观察到显著差异(p < 0.05)。Z350复合材料、浸渍玻璃纤维和中间粘合剂层的组合的FS最高。单独的Filtek P90的FS最低。除第5组外,所有组中复合材料的内聚破坏是主要破坏,在第5组中仅观察到复合材料与纤维之间的粘合破坏。
两种复合材料与玻璃纤维的FS均有显著提高。在复合材料堆积之前额外施加中间粘合剂层似乎会增加FS。纳米混合复合材料的FS高于硅氧烷基复合材料。