Jian Yu-Tao, Tang Tian-Yu, Swain Michael V, Wang Xiao-Dong, Zhao Ke
Institute of Stomatological Research, Sun Yat-sen University, Guangdong Provincial Key Laboratory of Stomatology, Guangzhou, China.
Department of Prosthodontics, Affiliated Stomatology Hospital of Kunming Medical University, Kunming, China.
Dent Mater. 2016 Dec;32(12):1453-1463. doi: 10.1016/j.dental.2016.06.007. Epub 2016 Sep 29.
The aim of this in vitro study was to evaluate the effect of core ceramic grinding on the fracture behaviour of bilayered zirconia under two loading schemes.
Interfacial surfaces of sandblasted zirconia disks (A) were ground with 80 (B), 120 (C) and 220 (D) grit diamond discs, respectively. Surface roughness and topographic analysis were performed using a confocal scanning laser microscope (CSLM) and a scanning electron microscopy (SEM). Relative monoclinic content was evaluated using X-ray diffraction analysis (XRD) then reevaluated after simulated veneer firing. Biaxial fracture strength (σ) and Weibull modulus (m) were calculated either with core in compression (subgroup Ac-Dc) or in tension (subgroup At-Dt). Facture surfaces were examined by SEM and energy dispersive X-ray spectroscopy (EDS). Maximum tensile stress at fracture was estimated by finite element analysis. Statistical data analysis was performed using Kruskal-Wallis and one-way ANOVA at a significance level of 0.05.
As grit size of the diamond disc increased, zirconia surface roughness decreased (p<0.001). Thermal veneering treatment reversed the transformation of monoclinic phase observed after initial grinding. No difference in initial (p=0.519 for subgroups Ac-Dc) and final fracture strength (p=0.699 for subgroups Ac-Dc; p=0.328 for subgroups At-Dt) was found among the four groups for both loading schemes. While coarse grinding slightly increased final fracture strength reliability (m) for subgroups Ac-Dc. Two different modes of fracture were observed according to which material was on the bottom surface. Components of the liner porcelain remained on the zirconia surface after fracture for all groups.
Technician grinding changed surface topography of zirconia ceramic material, but was not detrimental to the bilayered system strength after veneer application. Coarse grinding slightly improved the fracture strength reliability of the bilayered system tested with core in compression. It is recommended that veneering porcelain be applied directly after routine lab grinding of zirconia ceramic, and its application on rough zirconia cores may be preferred to enhance bond strength.
本体外研究旨在评估在两种加载方案下,核心陶瓷研磨对双层氧化锆断裂行为的影响。
分别用80目(B)、120目(C)和220目(D)的金刚石磨盘研磨喷砂氧化锆盘(A)的界面表面。使用共聚焦扫描激光显微镜(CSLM)和扫描电子显微镜(SEM)进行表面粗糙度和形貌分析。使用X射线衍射分析(XRD)评估相对单斜晶含量,然后在模拟饰面烧制后重新评估。双轴断裂强度(σ)和威布尔模量(m)通过核心受压(亚组Ac-Dc)或受拉(亚组At-Dt)来计算。通过SEM和能量色散X射线光谱(EDS)检查断裂表面。通过有限元分析估计断裂时的最大拉应力。使用Kruskal-Wallis检验和单因素方差分析进行统计数据分析,显著性水平为0.05。
随着金刚石磨盘粒度的增加,氧化锆表面粗糙度降低(p<0.001)。热饰面处理逆转了初始研磨后观察到的单斜晶相转变。对于两种加载方案,四组之间在初始断裂强度(亚组Ac-Dc,p=0.519)和最终断裂强度(亚组Ac-Dc,p=0.699;亚组At-Dt,p=0.328)方面均未发现差异。虽然粗磨略微提高了亚组Ac-Dc的最终断裂强度可靠性(m)。根据底部表面的材料不同,观察到两种不同的断裂模式。所有组断裂后,衬层瓷的成分仍留在氧化锆表面。
技师研磨改变了氧化锆陶瓷材料的表面形貌,但对饰面应用后的双层系统强度没有不利影响。粗磨略微提高了核心受压测试的双层系统的断裂强度可靠性。建议在对氧化锆陶瓷进行常规实验室研磨后直接施加饰面瓷,在粗糙的氧化锆核心上施加饰面瓷可能更有利于提高粘结强度。