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基于光纤傅里叶变换近红外光谱法和偏最小二乘回归法监测猕猴桃酒发酵过程中残余糖分和酒精度的可行性研究

A Feasibility Study on Monitoring Residual Sugar and Alcohol Strength in Kiwi Wine Fermentation Using a Fiber-Optic FT-NIR Spectrometry and PLS Regression.

作者信息

Wang Bingqian, Peng Bangzhu

机构信息

Key Laboratory of Environment Correlative Dietology, Ministry of Education, College of Food Science and Technology, Huazhong Agricultural Univ., 430070, Wuhan, Hubei, China.

出版信息

J Food Sci. 2017 Feb;82(2):358-363. doi: 10.1111/1750-3841.13604. Epub 2017 Jan 19.

Abstract

This work aims to investigate the potential of fiber-optic Fourier transform-near-infrared (FT-NIR) spectrometry associated with chemometric analysis, which will be applied to monitor time-related changes in residual sugar and alcohol strength during kiwi wine fermentation. NIR calibration models for residual sugar and alcohol strength during kiwi wine fermentation were established on the FT-NIR spectra of 98 samples scanned in a fiber-optic FT-NIR spectrometer, and partial least squares regression method. The results showed that R and root mean square error of cross-validation could achieve 0.982 and 3.81 g/L for residual sugar, and 0.984 and 0.34% for alcohol strength, respectively. Furthermore, crucial process information on kiwi must and wine fermentations provided by fiber-optic FT-NIR spectrometry was found to agree with those obtained from traditional chemical methods, and therefore this fiber-optic FT-NIR spectrometry can be applied as an effective and suitable alternative for analyses and monitoring of those processes. The overall results suggested that fiber-optic FT-NIR spectrometry is a promising tool for monitoring and controlling the kiwi wine fermentation process.

摘要

本研究旨在探讨光纤傅里叶变换近红外(FT-NIR)光谱法结合化学计量学分析的潜力,该方法将用于监测猕猴桃酒发酵过程中残余糖分和酒精度随时间的变化。利用光纤傅里叶变换近红外光谱仪扫描的98个样品的FT-NIR光谱,采用偏最小二乘回归法建立了猕猴桃酒发酵过程中残余糖分和酒精度的近红外校准模型。结果表明,残余糖分的相关系数R和交叉验证均方根误差分别可达0.982和3.81 g/L,酒精度的相关系数R和交叉验证均方根误差分别可达0.984和0.34%。此外,发现光纤FT-NIR光谱法提供的猕猴桃原酒和葡萄酒发酵的关键过程信息与传统化学方法获得的信息一致,因此这种光纤FT-NIR光谱法可作为这些过程分析和监测的有效且合适的替代方法。总体结果表明,光纤FT-NIR光谱法是监测和控制猕猴桃酒发酵过程的一种有前景的工具。

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