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2304双相不锈钢的应力腐蚀开裂——微观结构、残余应力及表面磨削影响

SCC of 2304 Duplex Stainless Steel-Microstructure, Residual Stress and Surface Grinding Effects.

作者信息

Zhou Nian, Peng Ru Lin, Schönning Mikael, Pettersson Rachel

机构信息

Department of Material Science, Dalarna University, SE-79188 Falun, and KTH, SE-10044 Stockholm, Sweden.

Department of Management and Engineering, Linköping University, SE-58183 Linköping, Sweden.

出版信息

Materials (Basel). 2017 Feb 23;10(3):221. doi: 10.3390/ma10030221.

Abstract

The influence of surface grinding and microstructure on chloride induced stress corrosion cracking (SCC) behavior of 2304 duplex stainless steel has been investigated. Grinding operations were performed both parallel and perpendicular to the rolling direction of the material. SCC tests were conducted in boiling magnesium chloride according to ASTM G36; specimens were exposed both without external loading and with varied levels of four-point bend loading. Residual stresses were measured on selected specimens before and after exposure using the X-ray diffraction technique. In addition, in-situ surface stress measurements subjected to four-point bend loading were performed to evaluate the deviation between the actual applied loading and the calculated values according to ASTM G39. Micro-cracks, initiated by grinding induced surface tensile residual stresses, were observed for all the ground specimens but not on the as-delivered surfaces. Loading transverse to the rolling direction of the material increased the susceptibility to chloride induced SCC. Grinding induced tensile residual stresses and micro-notches in the as-ground surface topography were also detrimental.

摘要

研究了表面磨削和微观结构对2304双相不锈钢氯化物诱导应力腐蚀开裂(SCC)行为的影响。磨削操作分别平行和垂直于材料的轧制方向进行。根据ASTM G36在沸腾的氯化镁中进行SCC试验;试样分别在无外部载荷和施加不同水平的四点弯曲载荷的情况下进行暴露。使用X射线衍射技术在暴露前后对选定的试样测量残余应力。此外,进行了四点弯曲载荷下的原位表面应力测量,以评估实际施加的载荷与根据ASTM G39计算的值之间的偏差。在所有磨削试样的表面均观察到由磨削引起的表面拉伸残余应力引发的微裂纹,而在交付状态的表面未观察到。垂直于材料轧制方向的加载增加了氯化物诱导SCC的敏感性。磨削引起的拉伸残余应力和磨削后表面形貌中的微缺口也有不利影响。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ae0a/5503411/36fa2c116ed1/materials-10-00221-g001.jpg

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