Department of Prosthodontics, School of Dentistry, Mashhad University of Medical Sciences, Mashhad, Iran.
J Prosthodont. 2019 Apr;28(4):e881-e885. doi: 10.1111/jopr.12651. Epub 2017 Sep 5.
To investigate the effect of neodymium-doped yttrium aluminum garnet (Nd:YAG) laser irradiation on the surface properties and bond strength of zirconia ceramics.
Forty-eight zirconia ceramic pieces (4 × 4 × 1 mm ) were divided into four groups according to surface treatment as follows: two control groups (no treatment) for resin bonding (CRC) and glass ionomer (GI) bonding (CGC); two laser treatment groups (Nd:YAG irradiation, 3 W, 200 MJ, 10 Hz, 180 μs) for resin bonding (LRC) and GI bonding (LGC). The ceramics in the control groups and the laser groups were distinguished by the application of different cements (resin cement and GI). Following surface treatments, the specimens were cemented to human dentin with resin cement and GI. After bonding, the shear bond strength (SBS) of the ceramic to dentin was measured, and the failure mode of each specimen was analyzed using a stereomicroscope. A one-way ANOVA compared the average bond strength of the four groups. Pairwise comparisons among the groups were performed using the Games-Howell test. The level of significance was set at 0.05.
The means (± standard deviation) of SBS values in the CRC, CGC, LRC, and LGC groups were 3.98 ± 1.10, 1.66 ± 0.59, 10.24 ± 2.46, and 2.21 ± 0.38 MPa, respectively. Data showed that the application of the Nd:YAG laser resulted in a significantly greater SBS of the resin cement to the zirconia ceramics (p < 0.001). The highest bond strength was recorded in the LRC group. In the CRC group, 75% of the failures were of the adhesive type, compared with 66.7% and 83.3% in the LRC and LGC groups, respectively. In the CGC group, all failures were adhesive.
Pretreatment of zirconia ceramic via Nd:YAG laser improves the bond strength of the resin cement to the zirconia ceramic. GI cement does not provide sufficient bond strength of zirconia ceramics to dentin.
研究掺钕钇铝石榴石(Nd:YAG)激光照射对氧化锆陶瓷表面性能和结合强度的影响。
将 48 个氧化锆陶瓷试件(4×4×1mm)分为 4 组,根据表面处理方式如下:树脂粘结(CRC)和玻璃离子粘结(CGC)的 2 个对照组(不处理);树脂粘结(LRC)和玻璃离子粘结(LGC)的 2 个激光处理组(Nd:YAG 激光照射,3W,200MJ,10Hz,180μs)。对照组和激光组通过应用不同的粘结剂(树脂粘结剂和玻璃离子)来区分。表面处理后,将试件用树脂粘结剂和玻璃离子粘结到牙本质上。粘结后,测量陶瓷与牙本质的剪切结合强度(SBS),并用立体显微镜分析每个试件的失效模式。采用单因素方差分析比较 4 组的平均结合强度。采用 Games-Howell 检验进行组间两两比较。显著性水平设为 0.05。
CRC、CGC、LRC 和 LGC 组的 SBS 值平均值(±标准差)分别为 3.98±1.10、1.66±0.59、10.24±2.46 和 2.21±0.38MPa。数据表明,Nd:YAG 激光的应用使树脂粘结剂与氧化锆陶瓷的 SBS 显著增加(p<0.001)。LRC 组的结合强度最高。在 CRC 组中,75%的失效为粘接力型,而在 LRC 和 LGC 组中分别为 66.7%和 83.3%。在 CGC 组中,所有的失效均为粘接力型。
Nd:YAG 激光预处理氧化锆陶瓷可提高树脂粘结剂与氧化锆陶瓷的粘结强度。玻璃离子粘结剂不能为氧化锆陶瓷与牙本质提供足够的粘结强度。