气相色谱/质谱法测定鲶鱼（鲇鱼）组织中的β-苯乙胺

Determination of beta-phenylethylamine in catfish (Parasilurus asotus) tissues by gas chromatography/mass spectrometry.

Kumazawa T, Suzuki O, Seno H, Hattori H

Department of Legal Medicine, Hamamatsu University School of Medicine, Japan.

Comp Biochem Physiol C Comp Pharmacol Toxicol. 1988;91(2):571-4.

Abstract

beta-Phenylethylamine (PEA) was detected and quantitated in tissues of the catfish, Parasilurus asotus, by very specific and sensitive gas chromatography/mass spectrometry. 2. The selected ion monitoring was made with a strong quasi-molecular ion of the pentafluoropropionic derivative of PEA in the positive chemical ionization mode. 3. PEA was found in all tissues tested ranging from 2.8 to 38.2 ng/g wet wt tissue. It was highest in the spinal cord, followed by the skin, brain and intestine.

摘要

通过非常特异且灵敏的气相色谱/质谱法，在鲶鱼（鲇鱼）组织中检测并定量了β-苯乙胺（PEA）。2. 在正化学电离模式下，以PEA的五氟丙酸衍生物的强准分子离子进行选择离子监测。3. 在所有测试组织中均发现了PEA，含量范围为2.8至38.2纳克/克湿重组织。其在脊髓中含量最高，其次是皮肤、大脑和肠道。