Rösslhuber R, Uykur E, Dressel M
1. Physikalisches Institut, Universität Stuttgart, Pfaffenwaldring 57, D-70569 Stuttgart, Germany.
Rev Sci Instrum. 2018 May;89(5):054708. doi: 10.1063/1.5030847.
We present the design, test, and performance of a piston type pressure cell for low-temperature dielectric measurements up to 10 kbar with particular emphasis on the electrical feedthrough for four coaxial cables and four conventional copper wires. The coaxial cables provide proper shielding of the applied test signal; a commercial continuous flow cryostat allows us to minimize the total cable length enabling temperature and pressure-dependent dielectric spectroscopy measurements down to 8 K and up to 5 MHz. We performed open compensation measurements, i.e., background measurements of the response originating from the pressure setup without a sample, to obtain its high frequency characteristics. The stray capacitance of the pressure setup is determined as C = 40 fF, making it possible to measure small single crystals with a weak dielectric response. The proper operation is verified by comparing measurements of a test sample in the pressure setup at ambient pressure and in a standard dielectric spectroscopy setup.
我们介绍了一种用于低温介电测量的活塞式压力传感器的设计、测试和性能,该测量可达10千巴,特别强调了用于四根同轴电缆和四根传统铜线的电馈通。同轴电缆为施加的测试信号提供了适当的屏蔽;商用连续流低温恒温器使我们能够最小化总电缆长度,从而实现温度和压力相关的介电谱测量,最低温度可达8 K,最高频率可达5 MHz。我们进行了开路补偿测量,即对无样品时压力装置产生的响应进行背景测量,以获得其高频特性。压力装置的杂散电容确定为C = 40 fF,这使得测量具有微弱介电响应的小单晶成为可能。通过比较在环境压力下压力装置中测试样品的测量结果与标准介电谱装置中的测量结果,验证了其正常运行。