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具有定制品质和功能特性的低血糖全印度醋栗(L.)糖果的优化与多变量加速保质期测试(MASLT)

Optimization and multivariate accelerated shelf life testing (MASLT) of a low glycemic whole jamun ( L.) confection with tailored quality and functional attributes.

作者信息

Sehwag Sneha, Upadhyay Rohit, Das Madhusweta

机构信息

Department of Agricultural and Food Engineering, Indian Institute of Technology Kharagpur, Kharagpur, West Bengal 721302 India.

出版信息

J Food Sci Technol. 2018 Dec;55(12):4887-4900. doi: 10.1007/s13197-018-3423-4. Epub 2018 Sep 19.

Abstract

An optimization and multivariate accelerated shelf-life testing (MASLT) was demonstrated to develop a low glycemic (GI) whole jamun ( L.) confection (WJC) with soft texture and fruity hedonics targeted for diabetic strata. The hydrocolloids viz., agar (1-3 g), pectin (1-3 g), and polydextrose (24-28 g) were optimized [mixture design (MD)] to obtain hydrocolloid mix (HM) with a soft texture. Next, whole jamun ingredients viz, jamun pulp (JP) (20-30 g), seed powder (JSP) (1-5 g), and HM (25-35 g) were optimized (MD + PCA) for satisfactory texture, total polyphenolic content (TPC), and fruity hedonics. The optimized WJC was assayed for GI and modelled by univariate kinetics and MASLT (10-45 °C/75% humidity/120 days). Using MASLT, the collated effects of quality attributes (anthocyanin content, TPC, moisture, hardness, and total color change) were extracted as principal components to estimate new stability parameters viz, multivariate rate constants ( ), acceleration factors ( ), activation energy ( ), and cut-off criterion. The optimized WJC contains 2.3 g agar, 1.9 g pectin, 27.2 g polydextrose, 26.4 g JP, and 2 g JSP and had satisfactory hardness (1007 g), TPC (2.8 mg gallic acid equivalents/g), and low GI value (48.6). The zero-order kinetic fitting of univariate versus MASLT resulted in , , and shelf life (10 °C) of 7.8 versus 6.2, 43.81 versus 39.22 kJ/mol and 175 versus 186 days, respectively. MASLT simplified the kinetic interpretations to a single variable by collating the useful information from critical quality parameters and predicted shelf life precisely than univariate kinetics.

摘要

已证明通过优化和多变量加速保质期测试(MASLT)来开发一种针对糖尿病患者群体的、质地柔软且具有水果风味的低血糖指数(GI)全印度醋栗(L.)糖食(WJC)。对水胶体,即琼脂(1 - 3克)、果胶(1 - 3克)和聚葡萄糖(24 - 28克)进行了优化[混合设计(MD)],以获得质地柔软的水胶体混合物(HM)。接下来,对全印度醋栗成分,即印度醋栗果肉(JP)(20 - 30克)、种子粉(JSP)(1 - 5克)和HM(25 - 35克)进行了优化(MD + PCA),以获得令人满意的质地、总多酚含量(TPC)和水果风味。对优化后的WJC进行了GI测定,并通过单变量动力学和MASLT(10 - 45°C/75%湿度/120天)进行建模。使用MASLT,将质量属性(花青素含量、TPC、水分、硬度和总颜色变化)的综合影响提取为主成分,以估计新的稳定性参数,即多变量速率常数( )、加速因子( )、活化能( )和截止标准。优化后的WJC含有2.3克琼脂、1.9克果胶、27.2克聚葡萄糖、26.4克JP和2克JSP,具有令人满意的硬度(1007克)、TPC(2.8毫克没食子酸当量/克)和低GI值(48.6)。单变量与MASLT的零级动力学拟合结果分别为 、 以及在10°C下的保质期为7.8天对6.2天、43.81千焦/摩尔对39.22千焦/摩尔和175天对186天。MASLT通过整理关键质量参数的有用信息,将动力学解释简化为单个变量,并且比单变量动力学更精确地预测了保质期。

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