Department of Cariology and Operative Dentistry, Graduate School of Medical and Dental Sciences, Tokyo Medical and Dental University, 1-5-45, Yushima, Bunkyo-ku, Tokyo 113-8549, Japan.
Department of Cariology and Operative Dentistry, Graduate School of Medical and Dental Sciences, Tokyo Medical and Dental University, 1-5-45, Yushima, Bunkyo-ku, Tokyo 113-8549, Japan.
Dent Mater. 2019 May;35(5):730-739. doi: 10.1016/j.dental.2019.02.025. Epub 2019 Feb 28.
OBJECTIVES: Translucent zirconia has brought the advantages such as less tooth preparation, biological compatibility, high strength, good mechanical properties, and less antagonist wear. This study's aim was to elucidate how clinically relevant surface treatments; alumina-abrasion and priming effect on bond strength of Y-PSZ in three different translucency grades after long-term water storage. MATERIALS AND METHODS: Three highly translucent Y-PSZ grades were ground flat with #600-grit SiC paper. Four different surface treatments (untreated, alumina blasting at 0.1 MPa or 0.2 MPa or 0.4 MPa) and two resin cements (PANAVIA V5 and PANAVIA SA CEMENT PLUS AUTOMIX) were tested. The bonded specimens were stored in water for 1 day, 30 days and 150 days and tensile bond strength (TBS) were measured with universal testing machine at a crosshead speed of 2 mm/min (n=10). The surface roughness (Sa) measurement and surface morphology analysis without alumina-blasting pressure (untreated) and with alumina-blasting pressures (0.1 MPa, 0.2 MPa and 0.4 MPa) for three different zirconia grades were evaluated with 3D-Laser Scanning Confocal Microscope. RESULTS: Different alumina-blasting pressures and different storage periods affected the bonding of resin cement to translucent zirconia. The Weibull moduli increased in some groups after 150 days storage. After 1 day and 30 days storage, 0.4 MPa alumina-blasting pressure provided superior bond strength, however, after 150 days, 0.2 MPa gave reliable and stable bond strength. SIGNIFICANCE: Alumina-blasting pressure of 0.2 MPa was the most effective for reliable and durable bonding performance to translucent zirconia after long-term water storage.
目的:透明氧化锆带来了更少的牙体预备、生物相容性、高强度、良好的机械性能和较少的对颌磨损等优势。本研究旨在阐明临床相关的表面处理方法,即氧化铝喷砂(压力分别为 0.1 MPa、0.2 MPa 和 0.4 MPa)和底涂处理对三种不同透明度氧化锆 Y-PSZ 在长期水储存后的粘结强度的影响。
材料与方法:将三种高透明度 Y-PSZ 级研磨至平整,并用#600 粒度 SiC 砂纸进行研磨。共测试了四种不同的表面处理方法(未处理、氧化铝喷砂压力分别为 0.1 MPa、0.2 MPa 和 0.4 MPa)和两种树脂水门汀(PANAVIA V5 和 PANAVIA SA CEMENT PLUS AUTOMIX)。粘结试件在水中储存 1 天、30 天和 150 天,然后在万能试验机上以 2mm/min 的十字头速度测量拉伸粘结强度(TBS)(n=10)。使用三维激光共聚焦显微镜评估未经氧化铝喷砂处理(未处理)和在三种不同氧化锆等级下使用氧化铝喷砂压力(0.1 MPa、0.2 MPa 和 0.4 MPa)的表面粗糙度(Sa)测量和表面形貌分析。
结果:不同的氧化铝喷砂压力和不同的储存时间影响树脂水门汀与透明氧化锆的粘结。一些组在 150 天储存后,韦布尔模数增加。在 1 天和 30 天储存后,0.4 MPa 氧化铝喷砂压力提供了更高的粘结强度,但在 150 天后,0.2 MPa 提供了可靠且稳定的粘结强度。
意义:在长期水储存后,0.2 MPa 的氧化铝喷砂压力对透明氧化锆的粘结性能最有效,可提供可靠且持久的粘结性能。
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