Calandri Michele, Yin Shuo, Aldwell Barry, Calignano Flaviana, Lupoi Rocco, Ugues Daniele
Dipartimento di Scienza Applicata e Tecnologia (DISAT), Politecnico di Torino, Corso Duca degli Abruzzi, 24, 10129 Turin, Italy.
Department of Mechanical and Manufacturing Engineering, Trinity College Dublin, The University of Dublin, Parsons Building, Dublin 2, Ireland.
Materials (Basel). 2019 Apr 19;12(8):1293. doi: 10.3390/ma12081293.
Nickel-based Inconel 718 is a very good candidate for selective laser melting (SLM). During the SLM process, Inconel 718 develops a complex and heterogeneous microstructure. A deep understanding of the microstructural features of the as-built SLM material is essential for the design of a proper post-process heat treatment. In this study, the microstructure of as-built SLM Inconel 718 was investigated at different length scales using optical microscopy (OM), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). Electron backscatter diffraction (EBSD) was also used to analyze the grain morphology and crystallographic texture. Grains elongated in the build direction and crossing several deposited layers were observed. The grains are not constrained by the laser tracks or by the melt pools, which indicates epitaxial growth controls the solidification. Each grain is composed of fine columnar dendrites that develop along one of their <100> axes oriented in the direction of the local thermal gradient. Consequently, prominent <100> crystallographic texture was observed and the dendrites tend to grow to the build direction or with occasional change of 90° at the edge of the melt pools. At the dendrite length scale, the microsegregation of the alloying elements, interdendritic precipitates, and dislocations was also detected.
镍基合金Inconel 718是选择性激光熔化(SLM)的理想材料。在SLM过程中,Inconel 718会形成复杂且不均匀的微观结构。深入了解增材制造的SLM材料的微观结构特征对于设计合适的后处理热处理至关重要。在本研究中,使用光学显微镜(OM)、扫描电子显微镜(SEM)和透射电子显微镜(TEM)在不同长度尺度下研究了增材制造的SLM Inconel 718的微观结构。电子背散射衍射(EBSD)也用于分析晶粒形态和晶体取向。观察到晶粒在堆积方向上伸长并穿过多个沉积层。晶粒不受激光轨迹或熔池的限制,这表明外延生长控制凝固过程。每个晶粒由沿其<100>轴之一生长的细柱状枝晶组成,该轴沿局部热梯度方向取向。因此,观察到明显的<100>晶体取向,并且枝晶倾向于向堆积方向生长,或者在熔池边缘偶尔发生90°的变化。在枝晶长度尺度上,还检测到合金元素的微观偏析、枝晶间析出物和位错。