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使用亲水性底漆粘结的正畸磨牙管剪切粘结强度的评估:一项体外研究。

Evaluation of shear bond strength of orthodontic molar tubes bonded using hydrophilic primers: An in vitro study.

作者信息

Hadrous Rima, Bouserhal Joseph, Osman Essam

机构信息

Beirut Arab university, faculty of dentistry, division of orthodontics, Beirut, Lebanon.

Beirut Arab university, Beirut, Lebanon; Boston university, Boston, USA; Saint-Joseph university of Beirut, Beirut, Lebanon.

出版信息

Int Orthod. 2019 Sep;17(3):461-468. doi: 10.1016/j.ortho.2019.06.006. Epub 2019 Jul 2.

Abstract

OBJECTIVE

To evaluate and compare the shear bond strength (SBS) of orthodontic molar tubes bonded using two hydrophilic primers along with a moisture tolerant adhesive system to dry and saliva-contaminated enamel surfaces; and to assess the mode of their bond failure.

MATERIALS AND METHODS

A total of 60 extracted human mandibular molars were randomly divided into three major groups according to the primer used, each consisting of 20 molars: XT group acts as a control and bonded with the conventional hydrophobic Transbond XT primer, OS group bonded with the hydrophilic Ortho Solo primer, AP group bonded with the hydrophilic Assure Plus all surface bonding resin. Each major group was further divided into two subgroups, of 10 molars each, according to presence or absence of saliva. All the specimens were thermocycled 500 cycles between 5̊ and 55°C. Shear forces were applied to the specimens with a universal testing machine at a crosshead speed of 1mm/min and SBS was measured in megapascals (MPa). The mode of failure was determined using the adhesive remnant index (ARI). Data were analysed using two-way analysis of variance (ANOVA) followed by univariate analysis and Bonferroni post hoc tests.

RESULTS

The three tested primers did not show a significant difference in the mean SBS in dry conditions (P=0.137); the mean SBS of OS and AP primers were 15.60±5.879MPa and 12.51±2.583MPa respectively which were comparable to that of the hydrophobic XT primer (12.76±2.952MPa). In saliva-contaminated conditions, the mean SBS values were 10.41±4.457MPa and 9.22±3.422MPa for OS and AP primers respectively, which were significantly higher than that of XT primer (4.82±2.050MPa) (P=0.004). When comparing the mean SBS for each group according to the bonding condition, it was significantly higher in dry bonding compared to saliva-contaminated bonding for the three primers; XT (P<0.001), OS (P=0.003) and AP (P=0.011). In the dry field, most of the bond failures of the three primers were adhesive (score 3), whereas in the saliva-contaminated field, most of the failures were cohesive (score 1).

CONCLUSION

Dry bonding yielded the highest SBS for the three primers. Saliva contamination significantly decreased the bond strength of both hydrophilic primers; however, the values were above the clinically acceptable limit. The hydrophilic primers tested in the present study can be successfully used for bonding orthodontic molar tubes under dry and saliva-contaminated enamel surface conditions.

摘要

目的

评估并比较两种亲水性底漆与一种耐湿粘结系统结合使用时,在干燥和唾液污染的牙釉质表面粘结正畸磨牙管的剪切粘结强度(SBS);并评估其粘结失败模式。

材料与方法

根据使用的底漆,将60颗拔除的人类下颌磨牙随机分为三大组,每组20颗磨牙:XT组作为对照组,使用传统的疏水性Transbond XT底漆粘结;OS组使用亲水性Ortho Solo底漆粘结;AP组使用亲水性Assure Plus全表面粘结树脂粘结。根据是否存在唾液,每个大组进一步分为两个亚组,每组10颗磨牙。所有标本在5̊和55°C之间进行500次热循环。使用万能试验机以1mm/min的十字头速度对标本施加剪切力,并以兆帕(MPa)为单位测量SBS。使用粘结残留指数(ARI)确定失败模式。数据采用双向方差分析(ANOVA),随后进行单因素分析和Bonferroni事后检验。

结果

在干燥条件下,三种测试底漆的平均SBS无显著差异(P=0.137);OS底漆和AP底漆的平均SBS分别为15.60±5.879MPa和12.51±2.583MPa,与疏水性XT底漆(12.76±2.952MPa)相当。在唾液污染条件下,OS底漆和AP底漆的平均SBS值分别为10.41±4.457MPa和9.22±3.422MPa,显著高于XT底漆(4.82±2.050MPa)(P=0.004)。根据粘结条件比较每组的平均SBS时,三种底漆在干燥粘结时均显著高于唾液污染粘结;XT(P<0.001)、OS(P=0.003)和AP(P=0.011)。在干燥环境中,三种底漆的大多数粘结失败为粘结性(评分为3),而在唾液污染环境中,大多数失败为内聚性(评分为1)。

结论

对于三种底漆,干燥粘结产生的SBS最高。唾液污染显著降低了两种亲水性底漆的粘结强度;然而,这些值高于临床可接受的限度。本研究中测试的亲水性底漆可成功用于在干燥和唾液污染的牙釉质表面条件下粘结正畸磨牙管。

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