Campos P H O V, Appoloni C R, Rizzutto M A, Leite A R, Assis R F, Santos H C, Silva T F, Rodrigues C L, Tabacniks M H, Added N
Instituto de Física, Universidade de São Paulo, Rua do Matão, Trav. R, 187, 05508-090, São Paulo, Brazil; Departamento de Física, Centro de Ciências Exatas, Universidade Estadual de Londrina, Londrina, Brazil.
Departamento de Física, Centro de Ciências Exatas, Universidade Estadual de Londrina, Londrina, Brazil.
Appl Radiat Isot. 2019 Oct;152:78-85. doi: 10.1016/j.apradiso.2019.06.018. Epub 2019 Jun 13.
This work presents the development of a portable system that allows 2D elemental mapping of large areas (maximum of 35.0 × 35.0 cm) by XRF. A measuring head, composed of an x-ray source and a detector, is mounted on a 3-axis stage with movement reproducibility better that 0.03 mm. The final elemental map resolution of 1.4 mm was experimentally determined in the best condition of collimation, and the same experiments indicate that the resolution is fully dominated by the x-ray beam spot size. The main goal of this new setup is to perform analyses of historical, archaeological and geological objects. Because it's lightweight, our setup has the potential to be of great utility for in situ analyses, given the great difficulty and high costs transporting the artifacts from the museum to a laboratory. The importance of this instrumentation is related to the need to identify the distribution of the chemical elements in large surface areas of cultural heritage objects by a nondestructive method.
这项工作展示了一种便携式系统的开发,该系统可通过X射线荧光光谱法对大面积区域(最大35.0×35.0厘米)进行二维元素映射。一个由X射线源和探测器组成的测量头安装在一个三轴工作台上,其运动重复性优于0.03毫米。在最佳准直条件下,通过实验确定最终元素映射分辨率为1.4毫米,相同实验表明该分辨率完全由X射线束光斑尺寸决定。这种新装置的主要目标是对历史、考古和地质物体进行分析。由于其重量轻,鉴于将文物从博物馆运到实验室存在很大困难且成本高昂,我们的装置有潜力在现场分析中发挥巨大作用。这种仪器的重要性在于需要通过无损方法识别文化遗产物体大表面积中化学元素的分布情况。