Advanced Photon Source, Argonne National Laboratory, 9700 S. Cass Avenue, Lemont, IL 60439, USA.
J Synchrotron Radiat. 2019 Nov 1;26(Pt 6):1924-1928. doi: 10.1107/S1600577519013328. Epub 2019 Oct 23.
Calibration of area detectors from powder diffraction standards is widely used at synchrotron beamlines. From a single diffraction image, it is not possible to determine both the sample-to-detector distance and the wavelength, but, with images taken from multiple positions along the beam direction and where the relative displacement is known, the sample-to-detector distance and wavelength can both be determined with good precision. An example calibration using the GSAS-II software package is presented.
从粉末衍射标准对面探测器进行定标在同步加速器光束线上被广泛应用。从单个衍射图像,无法同时确定样品到探测器的距离和波长,但通过沿着光束方向从多个位置采集图像,并已知相对位移,可以高精度地同时确定样品到探测器的距离和波长。本文介绍了使用 GSAS-II 软件包进行的校准示例。