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含甲烷水合物沉积物的三轴测试与孔隙尺度可视化的整合

Integration of triaxial testing and pore-scale visualization of methane hydrate bearing sediments.

作者信息

Seol Yongkoo, Lei Liang, Choi Jeong-Hoon, Jarvis Karl, Hill Daniel

机构信息

National Energy Technology Laboratory, U.S. Department of Energy, Morgantown, West Virginia 26507, USA.

出版信息

Rev Sci Instrum. 2019 Dec 1;90(12):124504. doi: 10.1063/1.5125445.

Abstract

Understanding mechanical interactions between hydrate and hosting sediments is critical for evaluating formation stability and associated environmental impacts of hydrate-bearing sediments during gas production. While core-scale studies of hydrate-bearing sediments are readily available and some explanations of observed results rely on pore-scale behavior of hydrate, actual pore-scale observations supporting the larger-scale phenomena are rarely available for hydrate-bearing sediments, especially with methane as guest molecules. The primary reasons for the scarcity include the challenge of developing tools for small-scale testing apparatus and pore-scale visualization capability. We present a testing assembly that combines pore-scale visualization and triaxial test capability of methane hydrate-bearing sediments. This testing assembly allows temperature regulation and independent control of four pressures: influent and effluent pore pressure, confining pressure, and axial pressure. Axial and lateral effective stresses can be applied independently to a 9.5 mm diameter and 19 mm long specimen while the pore pressure and temperature are controlled to maintain the stability of methane hydrate. The testing assembly also includes an X-ray transparent beryllium core holder so that 3D computed tomography scanning can be conducted during the triaxial loading. This testing assembly permits pore-scale exploration of hydrate-sediment interaction in addition to the traditional stress-strain relationship. Exemplary outcomes are presented to demonstrate applications of the testing assembly on geomechanical property estimations of methane-hydrate bearing sediments.

摘要

了解水合物与宿主沉积物之间的力学相互作用对于评估天然气生产过程中含天然气水合物沉积物的地层稳定性及相关环境影响至关重要。虽然关于含天然气水合物沉积物的岩心尺度研究已有不少,且对观测结果的一些解释依赖于水合物的孔隙尺度行为,但对于含天然气水合物沉积物,尤其是以甲烷作为客体分子的情况,支持更大尺度现象的实际孔隙尺度观测却很少见。这种稀缺的主要原因包括开发用于小型测试设备的工具以及孔隙尺度可视化能力方面的挑战。我们展示了一种测试装置,它结合了含甲烷天然气水合物沉积物的孔隙尺度可视化和三轴测试能力。该测试装置能够调节温度并独立控制四种压力:进水和出水孔隙压力、围压以及轴向压力。在控制孔隙压力和温度以维持甲烷水合物稳定性的同时,可以对直径9.5毫米、长度19毫米的试样独立施加轴向和侧向有效应力。该测试装置还包括一个X射线透明铍岩心夹持器,以便在三轴加载过程中进行三维计算机断层扫描。除了传统的应力 - 应变关系外,该测试装置还允许对水合物 - 沉积物相互作用进行孔隙尺度的探索。文中给出了示例性结果,以展示该测试装置在含甲烷天然气水合物沉积物地质力学性质估算方面的应用。

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