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焊后热处理对用过渡层法焊接的异种材料微观结构及电化学特性的影响

Effect of Post Weld Heat Treatment on the Microstructure and Electrochemical Characteristics of Dissimilar Material Welded by Butter Method.

作者信息

Masood Chaudry Umer, Ahmad Hafiz Waqar, Tariq Muhammad Rehan, Farooq Ameeq, Khan Muhammad Kashif, Sher Farooq, Zeb Hassan, Hamad Kotiba

机构信息

School of Advanced Materials Science & Engineering, Sungkyunkwan University, Suwon 16419, Korea.

School of mechanical Engineering, Sungkyunkwan University, Suwon 16419, Korea.

出版信息

Materials (Basel). 2020 Oct 12;13(20):4512. doi: 10.3390/ma13204512.

Abstract

In the present study, the effect of post weld heat treatment (PWHT) on the microstructure and corrosion kinetics of butter welded Nickel Alloy 617 and 12Cr steel was investigated. Buttering was carried out on the 12Cr side with the Thyssen 617 filler metal. Furthermore, post weld heat treatment (PWHT) was conducted at 730 °C with a holding time of 4 h followed by furnace cooling. Optical Microscopy (OM) was conducted to study the microstructural evolution in dissimilar material welding as a result of PWHT. Moreover, Scanning Electron Microscopy with energy dispersive spectroscopy (SEM-EDS) was employed to determine the elemental concentrations in all important regions of the butter weld before and after the PWHT. In addition, the effect of PWHT on the corrosion kinetics of the butter weld was also investigated by potentiodynamic polarization measurements in 5 wt.% NaCl + 0.5 wt.% CHCOOH electrolyte at room temperature, 30 °C, 50 °C and 70 °C. The corrosion activation parameters were also determined for both the samples by using Arrhenius plots. The results revealed the higher susceptibility of corrosion of the butter weld after PWHT, which was attributed to the reduced Cr content in the heat affected zone of the 12Cr region due to the sensitization effect of the heat treatment, resulting in higher corrosion rates.

摘要

在本研究中,研究了焊后热处理(PWHT)对镍基合金617与12Cr钢过渡堆焊焊缝微观结构及腐蚀动力学的影响。采用蒂森617填充金属在12Cr钢一侧进行过渡堆焊。此外,在730℃下进行焊后热处理(PWHT),保温4小时,随后炉冷。采用光学显微镜(OM)研究了焊后热处理导致的异种材料焊接微观结构演变。此外,利用扫描电子显微镜和能谱仪(SEM-EDS)测定了焊后热处理前后过渡堆焊焊缝所有重要区域的元素浓度。此外,还通过在室温、30℃、50℃和70℃下于5 wt.% NaCl + 0.5 wt.% CHCOOH电解液中进行动电位极化测量,研究了焊后热处理对过渡堆焊焊缝腐蚀动力学的影响。还通过使用阿累尼乌斯图为两个样品测定了腐蚀活化参数。结果表明,焊后热处理后过渡堆焊焊缝的腐蚀敏感性更高,这归因于由于热处理的敏化作用,12Cr区域热影响区中的Cr含量降低,导致腐蚀速率更高。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2383/7601325/6af26404c63c/materials-13-04512-g001.jpg

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