Ockenfels Till, Vewinger Frank, Weitz Martin
Institut für Angewandte Physik, Universität Bonn, Wegelerstr. 8, D-53115 Bonn, Germany.
Rev Sci Instrum. 2021 Jun 1;92(6):065109. doi: 10.1063/5.0047609.
We describe the design of a soldered sapphire optical viewport, which is useful for spectroscopic applications of samples at high temperatures and high pressures. The sapphire window is bonded via active soldering to a metal flange with a structure of two c-shaped rings made of different metallic materials in between, so as to mitigate thermally induced stress. A spectroscopic cell equipped with two of the optical viewports has been successfully operated with alkali metals in a noble gas environment at temperatures in the range of 20-450 °C at noble gas pressures from 10 mbar to 330 bars. In the upper pressure range, we observe a leakage rate smaller than our readout accuracy of 30 mbar per day.
我们描述了一种焊接蓝宝石光学视窗的设计,该视窗对于高温高压下样品的光谱应用很有用。蓝宝石窗口通过活性焊接与金属法兰相连,中间有两个由不同金属材料制成的C形环结构,以减轻热致应力。一个配备了两个这种光学视窗的光谱池已成功地在惰性气体环境中,于20至450°C的温度范围以及10毫巴至330巴的惰性气体压力下,与碱金属一起运行。在上限压力范围内,我们观察到泄漏率小于我们每天30毫巴的读出精度。