Medina Isabel, Deuerling Julian, Kumari Pooja, Scholl Stephan, Rädle Matthias
Center for Mass Spectrometry and Optical Spectroscopy, Mannheim University of Applied Sciences, Paul-Wittsack-Straße 10, 68163 Mannheim, Germany.
Technische Universität Braunschweig, Institute for Chemical and Thermal Process Engineering, Langer Kamp 7, 38106 Braunschweig, Germany.
Micromachines (Basel). 2021 Aug 10;12(8):940. doi: 10.3390/mi12080940.
The work presents an efficient and non-invasive method to visualize the local concentration and viscosity distribution of two miscible and non-reacting substances with a significant viscosity difference in a microchannel with a Y-shape cell. The proof-of-concept setup consists of a near-infrared (NIR) camera and cost-effective dome lighting with NIR light-emitting diodes (LED) covering the wavelength range of 1050 to 1650 nm. Absorption differences of glycerol and water and their mixtures with a mass fraction of glycerol from 0 to 0.95 gGlycgtotal-1 were analyzed in the NIR spectral area. The resulting measurement images were converted in a concentration profile by using absorbance calculated with Lambert-Beer law. A linear behavior between the concentration and the absorption coefficient is demonstrated. The result of local concentration in mass fraction was used to determine the local viscosity and illustrated as distribution images. By variating the fluid parameters, the influences of the highly different original viscosities in the mixing procedure were investigated and visualized.
这项工作提出了一种高效且非侵入性的方法,用于在具有Y形单元的微通道中可视化两种可混溶且不发生反应、粘度差异显著的物质的局部浓度和粘度分布。概念验证装置由一台近红外(NIR)相机和具有成本效益的圆顶照明组成,该照明采用覆盖1050至1650 nm波长范围的近红外发光二极管(LED)。在近红外光谱区域分析了甘油和水及其甘油质量分数从0到0.95 gGlycgtotal-1的混合物的吸收差异。通过使用根据朗伯-比尔定律计算的吸光度,将所得测量图像转换为浓度分布曲线。证明了浓度与吸收系数之间的线性关系。质量分数局部浓度的结果用于确定局部粘度,并以分布图像的形式呈现。通过改变流体参数,研究并可视化了混合过程中原始粘度差异极大所产生的影响。