Li Shaohua, Jiang Wenchun, Xie Xuefang, Dong Zhilong
State Key Laboratory of Heavy Oil Processing, College of New Energy, China University of Petroleum (East China), Qingdao 266580, China.
Materials (Basel). 2021 Sep 26;14(19):5594. doi: 10.3390/ma14195594.
Austenite and duplex stainless steels are widely used in engineering, and the latter exhibits a more excellent combination of mechanical properties and corrosion resistance due to the coexistence of austenite and ferrite and higher nitrogen. However, fatigue failure still threatens their structural integrity. A comprehensive comparison of their cyclic deformation behavior is a major foundation to understand the role of duplex-phase microstructure and nitrogen in the safety assessment of engineering components. Thus, in this paper, the cyclic deformation behavior of fully-austenitic stainless steel 316L and duplex stainless steel 2205 was studied by a series of low cycle fatigue tests with various strain amplitudes, loading rates and tensile holding. A theoretical mechanism diagram of the interaction between nitrogen and dislocation movements during cyclic loads was proposed. Results show that the cyclic stress response of 2205 was the primary cyclic hardening, followed by a long-term cyclic softening regardless of strain amplitudes and rates, while an additional secondary hardening was observed for 316L at greater strain amplitudes. Cyclic softening of 2205 was restrained under slower strain rates or tensile holding due to the interaction between nitrogen and dislocations. The cyclic plasticity of 2205 started within the austenite, and gradually translated into the ferrite with the elevation of the cyclic amplitude, which lead to a decreased hardening ratio with the increase in amplitude and a shorter fatigue life for a given smaller plastic strain amplitude.
奥氏体不锈钢和双相不锈钢在工程领域有着广泛应用,由于奥氏体和铁素体共存以及氮含量较高,后者表现出更为优异的力学性能与耐腐蚀性组合。然而,疲劳失效仍对其结构完整性构成威胁。全面比较它们的循环变形行为是理解双相组织微观结构和氮在工程部件安全评估中作用的重要基础。因此,本文通过一系列不同应变幅值、加载速率和拉伸保持的低周疲劳试验,研究了全奥氏体不锈钢316L和双相不锈钢2205的循环变形行为。提出了循环载荷作用下氮与位错运动相互作用的理论机理图。结果表明,无论应变幅值和加载速率如何,2205的循环应力响应先是主要的循环硬化,随后是长期的循环软化,而在较大应变幅值下,316L还出现了额外的二次硬化。由于氮与位错之间的相互作用,在较低应变速率或拉伸保持条件下,2205的循环软化受到抑制。2205的循环塑性从奥氏体内部开始,随着循环幅值的升高逐渐转移到铁素体中,这导致随着幅值增加硬化率降低,对于给定的较小塑性应变幅值,疲劳寿命缩短。