Buj-Corral Irene, Vidal Daniel, Tejo-Otero Aitor, Padilla José Antonio, Xuriguera Elena, Fenollosa-Artés Felip
Department of Mechanical Engineering, School of Engineering of Barcelona (ETSEIB), Universitat Politècnica de Catalunya, Av. Diagonal, 647, 08028 Barcelona, Spain.
Centre CIM, Universitat Politècnica de Catalunya (CIM UPC), Carrer de Llorens i Artigas, 12, 08028 Barcelona, Spain.
Nanomaterials (Basel). 2021 Nov 3;11(11):2942. doi: 10.3390/nano11112942.
The main aim of the present paper is to study and analyze surface roughness, shrinkage, porosity, and mechanical strength of dense yttria-stabilized zirconia (YSZ) samples obtained by means of the extrusion printing technique. In the experiments, both print speed and layer height were varied, according to a 2 factorial design. Cuboid samples were defined, and three replicates were obtained for each experiment. After sintering, the shrinkage percentage was calculated in width and in height. Areal surface roughness, S, was measured on the lateral walls of the cuboids, and total porosity was determined by means of weight measurement. The compressive strength of the samples was determined. The lowest S value of 9.4 μm was obtained with low layer height and high print speed. Shrinkage percentage values ranged between 19% and 28%, and porosity values between 12% and 24%, depending on the printing conditions. Lowest porosity values correspond to low layer height and low print speed. The same conditions allow obtaining the highest average compressive strength value of 176 MPa, although high variability was observed. For this reason, further research will be carried out about mechanical strength of ceramic 3D printed samples. The results of this work will help choose appropriate printing conditions extrusion processes for ceramics.
本文的主要目的是研究和分析通过挤压印刷技术获得的致密氧化钇稳定氧化锆(YSZ)样品的表面粗糙度、收缩率、孔隙率和机械强度。在实验中,根据二因素设计改变打印速度和层高。定义了长方体样品,每个实验获得三个重复样品。烧结后,计算宽度和高度方向的收缩率。在长方体的侧壁上测量表面粗糙度S,并通过重量测量确定总孔隙率。测定样品的抗压强度。在低层高和高打印速度下获得了最低的S值9.4μm。收缩率值在19%至28%之间,孔隙率值在12%至24%之间,这取决于打印条件。最低孔隙率值对应低层高和低打印速度。相同条件下可获得最高平均抗压强度值176MPa,尽管观察到高变异性。因此,将对陶瓷3D打印样品的机械强度进行进一步研究。这项工作的结果将有助于为陶瓷挤压工艺选择合适的打印条件。