Zurutuza Irati, Isasti Nerea, Detemple Eric, Schwinn Volker, Mohrbacher Hardy, Uranga Pello
Materials and Manufacturing Division, CEIT-Basque Research and Technology Alliance (BRTA), 20018 Donostia-Saint Sebastian, Basque Country, Spain.
Mechanical and Materials Engineering Department, Universidad de Navarra, Tecnun, 20018 Donostia-Saint Sebastian, Basque Country, Spain.
Materials (Basel). 2022 Feb 15;15(4):1424. doi: 10.3390/ma15041424.
The dynamic recrystallization behavior of ultra-high strength boron-microalloyed steels optionally alloyed with niobium and molybdenum is analyzed in this paper. Multipass torsion tests were performed to simulate plate rolling conditions followed by direct quenching. The influence of alloy composition on the transformed microstructure was evaluated by means of EBSD, thereby characterizing the morphology of the austenite grain morphology after roughing and finishing passes. The results indicated that for Nb-microalloyed steel, partial dynamic recrystallization occurred and resulted in local clusters of fine-sized equiaxed grains dispersed within the pancaked austenitic structure. A recrystallized austenite fraction appeared and transformed into softer phase constituents after direct quenching. The addition of Mo was shown to be an effective means of suppressing dynamic recrystallization. This effect of molybdenum in addition to its established hardenability effects hence safeguards the formation of fully martensitic microstructures, particularly in direct quenching processes. Additionally, the circumstances initiating dynamic recrystallization were studied in more detail, and the interference of the various alloying elements with the observed phenomena and the potential consequences of dynamic recrystallization before quenching are discussed.
本文分析了超高强度硼微合金钢(可选地与铌和钼合金化)的动态再结晶行为。进行多道次扭转试验以模拟板材轧制条件,随后直接淬火。通过电子背散射衍射(EBSD)评估合金成分对转变后的微观组织的影响,从而表征粗轧和精轧道次后奥氏体晶粒形态的形貌。结果表明,对于铌微合金钢,发生了部分动态再结晶,并导致在扁平状奥氏体组织中分散着局部细小等轴晶粒簇。直接淬火后出现了再结晶奥氏体分数,并转变为较软的相组成。结果表明,添加钼是抑制动态再结晶的有效手段。钼的这种作用除了其已确定的淬透性作用外,因此有助于形成完全马氏体微观组织,特别是在直接淬火过程中。此外,更详细地研究了引发动态再结晶的情况,并讨论了各种合金元素对观察到的现象的干扰以及淬火前动态再结晶的潜在后果。