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蒲桃[(L.)Skeels]葡萄酒中气味活性挥发性化合物的表征

Characterization of odor-active volatile compounds of jambolan [ (L.) Skeels] wine.

作者信息

Pino Jorge A, Espinosa Sixsy, Duarte Cira

机构信息

Department of Aromas, Food Industry Research Institute, Carretera a Guatao km 3 ½, POB 19200, Havana, Cuba.

Department of Foods, Pharmacy and Food Institute, Havana, Cuba.

出版信息

J Food Sci Technol. 2022 Apr;59(4):1529-1537. doi: 10.1007/s13197-021-05163-9. Epub 2021 Jun 19.

Abstract

Volatile constituents in jambolan [ (L.) Skeels] wine were isolated by headspace-solid phase microextraction (HS-SPME) and analyzed by gas chromatography-flame ionization detector (GC-FID), gas chromatography-mass spectrometry (GC-MS), and gas chromatography-olfactometry (GC-O). The composition of the jambolan wine included 52 esters, 20 terpenes, 13 alcohols, 12 acids, 11 aldehydes, 4 ketones, 4 oxides, and 5 miscellaneous compounds. Aroma extract dilution analysis and odor activity units were used for the determination of odor-active compounds. A total of 19 odor-active compounds were found as odor-active volatiles, from which ()-β-ionone, phenylacetaldehyde, ethyl acetate, ethyl hexanoate, and ethyl benzoate were the most important. The similar results of the GC-O and OAV approaches suggests that HS-SPME-GC-O could be used as a fast and simple tool to quality control of the jambolan wine aroma.

摘要

采用顶空固相微萃取(HS-SPME)法分离毛叶枣[(L.)Skeels]葡萄酒中的挥发性成分,并通过气相色谱-火焰离子化检测器(GC-FID)、气相色谱-质谱联用仪(GC-MS)和气相色谱-嗅觉测量法(GC-O)进行分析。毛叶枣葡萄酒的成分包括52种酯类、20种萜类、13种醇类、12种酸类、11种醛类、4种酮类、4种氧化物和5种其他化合物。采用香气提取物稀释分析和气味活性单位来测定气味活性化合物。共发现19种气味活性化合物为挥发性气味活性物质,其中()-β-紫罗兰酮、苯乙醛、乙酸乙酯、己酸乙酯和苯甲酸乙酯最为重要。GC-O和OAV方法的相似结果表明,HS-SPME-GC-O可作为一种快速简便的工具用于毛叶枣葡萄酒香气的质量控制。

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