Xu Zhichao, Yang Wenju, Fan Jianfeng, Wu Tao, Gao Zeng
School of Materials Science and Engineering, Henan Polytechnic University, Jiaozuo 454003, China.
Key Laboratory of Interface Science and Engineering in Advanced Materials, Ministry of Education, Taiyuan University of Technology, Taiyuan 030024, China.
Materials (Basel). 2022 Apr 27;15(9):3156. doi: 10.3390/ma15093156.
In the present work, the microstructure and mechanical properties of Ti-6Al-4V alloy during multidirectional isothermal forging (MDIF) were systematically investigated. The evolution of the microstructure and texture of Ti-6Al-4V alloy during MDIF was studied using TEM and electron backscattered diffraction (EBSD). The experiment results showed that the grain size decreased with the increase in cumulative strain, especially in the easy deformation zone. After four deformation cycles, a homogeneous equiaxed grained microstructure with an average grain size of 0.14 μm was achieved. The texture changes of the alloy were studied in detail. After one cycle of MDIF, the texture was mainly composed of (0002) [01 10], and the Euler angles were (8°, 30°, 30°). The density of texture decreased with the increase in loading cycle, but the dispersion of texture increased. After four cycles of MDIF, the non-basal texture (1010) <1102> texture was observed, and the Euler angles were (82°, 33°, 0°). The highest achieved mechanical properties for Ti-6Al-4V alloy in the MDIF condition were a yield strength 900 MPa, ultimate tensile strength of 921 MPa, and an elongation of 12.1% at room temperature. The increase in MDIF cycles improved the hardness of the alloy. The significant improvement in mechanical properties was attributed to the ultrafine-grained microstructure.
在本研究中,系统地研究了Ti-6Al-4V合金在多向等温锻造(MDIF)过程中的微观结构和力学性能。利用透射电子显微镜(TEM)和电子背散射衍射(EBSD)研究了Ti-6Al-4V合金在MDIF过程中微观结构和织构的演变。实验结果表明,晶粒尺寸随着累积应变的增加而减小,尤其是在易变形区。经过四个变形循环后,获得了平均晶粒尺寸为0.14μm的均匀等轴晶微观结构。详细研究了合金的织构变化。MDIF一个循环后,织构主要由(0002)[01 10]组成,欧拉角为(8°, 30°, 30°)。织构密度随着加载循环次数的增加而降低,但织构的弥散度增加。MDIF四个循环后,观察到非基面织构(1010)<1102>织构,欧拉角为(82°, 33°, 0°)。在MDIF条件下,Ti-6Al-4V合金获得的最高力学性能为室温下屈服强度900MPa、抗拉强度921MPa和伸长率12.1%。MDIF循环次数的增加提高了合金的硬度。力学性能的显著提高归因于超细晶粒微观结构。