Reinhard Christina, Drakopoulos Michael, Charlesworth Christopher M, James Andrew, Patel Hiten, Tutthill Paul, Crivelli Davide, Deyhle Hans, Ahmed Sharif I
Diamond Light Source, Harwell Science and Innovation Campus, Didcot OX11 0DE, United Kingdom.
NSLS-II, Brookhaven National Laboratory, Upton, NY 11973, USA.
J Synchrotron Radiat. 2022 Jul 1;29(Pt 4):1004-1013. doi: 10.1107/S1600577522006300. Epub 2022 Jun 27.
The DIAD beamline for Dual Imaging and Diffraction at Diamond Light Source has opted to use an industrial robot to position its Dectris Pilatus 2M CdTe diffraction detector. This setup was chosen to enable flexible positioning of the detector in a quarter-sphere around the sample position whilst reliably holding the large weight of 139 kg of detector, detector mount and cabling in a stable position. Metrology measurements showed that the detector can be positioned with a linear repeatability of <19.7 µm and a rotational repeatability of <16.3 µrad. The detector position stays stable for a 12 h period with <10.1 µm of movement for linear displacement and <3.8 µrad for rotational displacement. X-ray diffraction from calibration samples confirmed that the robot is sufficiently stable to resolve lattice d-spacings within the instrumental broadening given by detector position and beam divergence.
位于钻石光源的用于双成像和衍射的DIAD光束线选择使用工业机器人来定位其Dectris Pilatus 2M碲化镉衍射探测器。选择这种设置是为了使探测器能够在围绕样品位置的四分之一球体内灵活定位,同时可靠地将重达139千克的探测器、探测器支架和电缆保持在稳定位置。计量测量表明,探测器的线性重复定位精度可达<19.7 μm,旋转重复定位精度可达<16.3 µrad。探测器位置在12小时内保持稳定,线性位移移动<10.1 μm,旋转位移移动<3.8 µrad。校准样品的X射线衍射证实,在探测器位置和光束发散所导致的仪器展宽范围内,机器人足够稳定,能够分辨晶格d间距。